tert-butyl 5-amino-2-methylthio-4-(3-(p-nitro-phenoxcarbonylamino)-phenyl)-thieno-[2,3-d]pyrimidine-6-carboxamide

Base Information

• Chemical Name: tert-butyl 5-amino-2-methylthio-4-(3-(p-nitro-phenoxcarbonylamino)-phenyl)-thieno-[2,3-d]pyrimidine-6-carboxamide
• CAS No.: 405891-10-3
• Molecular Formula: C₂₅H₂₄N₆O₅S₂
• Molecular Weight: 552.635

Synonyms:tert-butyl 5-amino-2-methylthio-4-(3-(p-nitro-phenoxcarbonylamino)-phenyl)-thieno-[2,3-d]pyrimidine-6-carboxamide

Chemical Property of tert-butyl 5-amino-2-methylthio-4-(3-(p-nitro-phenoxcarbonylamino)-phenyl)-thieno-[2,3-d]pyrimidine-6-carboxamide

Chemical Property:

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Technology Process of tert-butyl 5-amino-2-methylthio-4-(3-(p-nitro-phenoxcarbonylamino)-phenyl)-thieno-[2,3-d]pyrimidine-6-carboxamide

There total 1 articles about tert-butyl 5-amino-2-methylthio-4-(3-(p-nitro-phenoxcarbonylamino)-phenyl)-thieno-[2,3-d]pyrimidine-6-carboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

5-amino-4-(3-aminophenyl)-N-(tert-butyl)-2-(methylthio)thieno[2,3-d]pyrimidine-6-carboxamide (301847-69-8) + 4-Nitrophenyl chloroformate (7693-46-1) → tert-butyl 5-amino-2-methylthio-4-(3-(p-nitro-phenoxcarbonylamino)-phenyl)-thieno-[2,3-d]pyrimidine-6-carboxamide (405891-10-3)

Guidance literature:

In dichloromethane; at 20 ℃; for 1h;

Reference yield:

morpholine (110-91-8,99108-56-2) + tert-butyl 5-amino-2-methylthio-4-(3-(p-nitro-phenoxcarbonylamino)-phenyl)-thieno-[2,3-d]pyrimidine-6-carboxamide (405891-10-3) → tert-butyl 5-amino-2-methylthio-4-(3-(morpholin-4-yl)-carbonylamino-phenyl)-thieno[2,3-d]pyrimidine-6-carboxamide

Guidance literature:

With N-ethyl-N,N-diisopropylamine; In dichloromethane; at 20 ℃;

Reference yield:

1,2,3,6-tetrahydropyridine (694-05-3) + tert-butyl 5-amino-2-methylthio-4-(3-(p-nitro-phenoxcarbonylamino)-phenyl)-thieno-[2,3-d]pyrimidine-6-carboxamide (405891-10-3) → tert-butyl 5-amino-2-methylthio-4-(3-(1,2,3,6-tetrahydropyridinocarbonylamino)-phenyl)-thieno[2,3-d]pyrimidine-6-carboxamide

Guidance literature:

With urea;

upstream raw materials:

5-amino-4-(3-aminophenyl)-N-(tert-butyl)-2-(methylthio)thieno[2,3-d]pyrimidine-6-carboxamide

4-Nitrophenyl chloroformate

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