2,2'-(4-((5-cyano-1-(2-ethylhexyl)-2-hydroxy-4-methyl-6-oxo-1,6-dihydropyridin-3-yl)diazenyl)phenylsulfonylazanediyl)bis(ethane-2,1-diyl)diacrylate

Base Information

Chemical Name:2,2'-(4-((5-cyano-1-(2-ethylhexyl)-2-hydroxy-4-methyl-6-oxo-1,6-dihydropyridin-3-yl)diazenyl)phenylsulfonylazanediyl)bis(ethane-2,1-diyl)diacrylate
CAS No.:1357264-91-5
Molecular Formula:C₃₁H₃₉N₅O₈S
Molecular Weight:641.745
Hs Code.:

2,2'-(4-((5-cyano-1-(2-ethylhexyl)-2-hydroxy-4-methyl-6-oxo-1,6-dihydropyridin-3-yl)diazenyl)phenylsulfonylazanediyl)bis(ethane-2,1-diyl)diacrylate

Synonyms:2,2'-(4-((5-cyano-1-(2-ethylhexyl)-2-hydroxy-4-methyl-6-oxo-1,6-dihydropyridin-3-yl)diazenyl)phenylsulfonylazanediyl)bis(ethane-2,1-diyl)diacrylate

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Chemical Property of 2,2'-(4-((5-cyano-1-(2-ethylhexyl)-2-hydroxy-4-methyl-6-oxo-1,6-dihydropyridin-3-yl)diazenyl)phenylsulfonylazanediyl)bis(ethane-2,1-diyl)diacrylate

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Technology Process of 2,2'-(4-((5-cyano-1-(2-ethylhexyl)-2-hydroxy-4-methyl-6-oxo-1,6-dihydropyridin-3-yl)diazenyl)phenylsulfonylazanediyl)bis(ethane-2,1-diyl)diacrylate

There total 3 articles about 2,2'-(4-((5-cyano-1-(2-ethylhexyl)-2-hydroxy-4-methyl-6-oxo-1,6-dihydropyridin-3-yl)diazenyl)phenylsulfonylazanediyl)bis(ethane-2,1-diyl)diacrylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 20.0%

: 1357264-82-4
4-((5-cyano-1-(2-ethylhexyl)-2-hydroxy-4-methyl-6-oxo-1,6-dihydropyridin-3-yl)diazenyl)-N,N-bis(2-hydroxyethyl)benzenesulfonamide

: 625-36-5
2-chloropropionyl chloride

: 1357264-91-5
2,2'-(4-((5-cyano-1-(2-ethylhexyl)-2-hydroxy-4-methyl-6-oxo-1,6-dihydropyridin-3-yl)diazenyl)phenylsulfonylazanediyl)bis(ethane-2,1-diyl)diacrylate

Guidance literature:: With triethylamine; at 30 ℃;

Reference yield:

: 121-60-8
p-acetylaminobenzenesulfonyl chloride

: 1357264-91-5
2,2'-(4-((5-cyano-1-(2-ethylhexyl)-2-hydroxy-4-methyl-6-oxo-1,6-dihydropyridin-3-yl)diazenyl)phenylsulfonylazanediyl)bis(ethane-2,1-diyl)diacrylate

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium hydrogencarbonate / acetone / 3 h / 20 °C

2.1: hydrogenchloride / water / 1.5 h / 85 - 95 °C

2.2: 0.75 h / 5 °C

2.3: 0.5 h / 20 °C / pH 2 - 3

3.1: triethylamine / 30 °C

With hydrogenchloride; sodium hydrogencarbonate; triethylamine; In water; acetone;

Reference yield:

: 17262-65-6
N-(4-(N,N-bis(2-hydroxyethyl)sulfamoyl)phenyl)acetamide

: 1357264-91-5
2,2'-(4-((5-cyano-1-(2-ethylhexyl)-2-hydroxy-4-methyl-6-oxo-1,6-dihydropyridin-3-yl)diazenyl)phenylsulfonylazanediyl)bis(ethane-2,1-diyl)diacrylate

Guidance literature:: Multi-step reaction with 2 steps

1.1: hydrogenchloride / water / 1.5 h / 85 - 95 °C

1.2: 0.75 h / 5 °C

1.3: 0.5 h / 20 °C / pH 2 - 3

2.1: triethylamine / 30 °C

With hydrogenchloride; triethylamine; In water;