1,2-di-O-acetyl-5-O-benzoyl-3-deoxy-3-ethoxycarbonylmethyl-D-ribofuranose

Base Information

Chemical Name:1,2-di-O-acetyl-5-O-benzoyl-3-deoxy-3-ethoxycarbonylmethyl-D-ribofuranose
CAS No.:1173826-12-4
Molecular Formula:C₂₀H₂₄O₉
Molecular Weight:408.405
Hs Code.:

Synonyms:1,2-di-O-acetyl-5-O-benzoyl-3-deoxy-3-ethoxycarbonylmethyl-D-ribofuranose

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1,2-di-O-acetyl-5-O-benzoyl-3-deoxy-3-ethoxycarbonylmethyl-D-ribofuranose

Chemical Property:

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Technology Process of 1,2-di-O-acetyl-5-O-benzoyl-3-deoxy-3-ethoxycarbonylmethyl-D-ribofuranose

There total 1 articles about 1,2-di-O-acetyl-5-O-benzoyl-3-deoxy-3-ethoxycarbonylmethyl-D-ribofuranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 108-24-7
acetic anhydride

: ((3aR,5S,6R,6aR)-6-(2-ethoxy-2-oxoethyl)-2,2-dimethyltetrahydrofuro[2,3-d][1,3]dioxol-5-yl)methyl benzoate

: 1173826-12-4
1,2-di-O-acetyl-5-O-benzoyl-3-deoxy-3-ethoxycarbonylmethyl-D-ribofuranose

Guidance literature:: With methanesulfonic acid; acetic acid; at 20 ℃; Cooling with ice;
DOI:10.1134/S1068162009010099

Reference yield: 84.0%

: 1173826-12-4
1,2-di-O-acetyl-5-O-benzoyl-3-deoxy-3-ethoxycarbonylmethyl-D-ribofuranose

: 71-30-7
Cytosine

: 1173826-16-8
2'-O-acetyl-5'-O-benzoyl-3'-deoxy-3'-ethoxycarbonylmethyl-cytidine

Guidance literature:: Cytosine; With N,O-bis-(trimethylsilyl)-acetamide; In acetonitrile; at 50 ℃;

1,2-di-O-acetyl-5-O-benzoyl-3-deoxy-3-ethoxycarbonylmethyl-D-ribofuranose; With trimethylsilyl trifluoromethanesulfonate; In acetonitrile; for 4h; Reflux;

With water; sodium hydrogencarbonate; In acetonitrile; for 0.5h; Cooling; Saturated solution;
DOI:10.1134/S1068162009010099

Reference yield: 81.0%

: 1173826-12-4
1,2-di-O-acetyl-5-O-benzoyl-3-deoxy-3-ethoxycarbonylmethyl-D-ribofuranose

: 65-71-4,28806-14-6,691841-57-3
thymin

: 1173826-14-6
2'-O-acetyl-5'-O-benzoyl-3'-deoxy-3'-ethoxycarbonylmethylribothymidine

Guidance literature:: thymin; With N,O-bis-(trimethylsilyl)-acetamide; In acetonitrile; at 50 ℃;

1,2-di-O-acetyl-5-O-benzoyl-3-deoxy-3-ethoxycarbonylmethyl-D-ribofuranose; With trimethylsilyl trifluoromethanesulfonate; In acetonitrile; for 4h; Reflux;

With water; sodium hydrogencarbonate; In acetonitrile; for 0.5h; Cooling; Saturated solution;
DOI:10.1134/S1068162009010099