RS-tert-butyldimethylsilyl 1-<4-(2-methoxyethoxy)methoxyphenyl>ethyl ether

Base Information

Chemical Name:RS-tert-butyldimethylsilyl 1-<4-(2-methoxyethoxy)methoxyphenyl>ethyl ether
CAS No.:135921-84-5
Molecular Formula:C₁₈H₃₂O₄Si
Molecular Weight:340.535
Hs Code.:

Synonyms:RS-tert-butyldimethylsilyl 1-<4-(2-methoxyethoxy)methoxyphenyl>ethyl ether

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of RS-tert-butyldimethylsilyl 1-<4-(2-methoxyethoxy)methoxyphenyl>ethyl ether

Chemical Property:

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Technology Process of RS-tert-butyldimethylsilyl 1-<4-(2-methoxyethoxy)methoxyphenyl>ethyl ether

There total 3 articles about RS-tert-butyldimethylsilyl 1-<4-(2-methoxyethoxy)methoxyphenyl>ethyl ether which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 135921-81-2
(RS)-1-<4-(2-methoxyethoxy)methoxyphenyl>ethanol

: 18162-48-6
tert-butyldimethylsilyl chloride

: 135921-84-5
RS-tert-butyldimethylsilyl 1-<4-(2-methoxyethoxy)methoxyphenyl>ethyl ether

Guidance literature:: With 1H-imidazole; In N,N-dimethyl-formamide;

Reference yield:

: 84775-31-5
1-(4-((2-methoxyethoxy)methoxy)phenyl)ethanone

: 135921-84-5
RS-tert-butyldimethylsilyl 1-<4-(2-methoxyethoxy)methoxyphenyl>ethyl ether

Guidance literature:: Multi-step reaction with 2 steps

1: 97 percent / NaBH₄ / aq. ethanol

2: 98 percent / imidazole / dimethylformamide

With 1H-imidazole; sodium tetrahydroborate; In ethanol; N,N-dimethyl-formamide;

Reference yield:

: 99-93-4
4-Hydroxyacetophenone

: 135921-84-5
RS-tert-butyldimethylsilyl 1-<4-(2-methoxyethoxy)methoxyphenyl>ethyl ether

Guidance literature:: Multi-step reaction with 3 steps

1: 100 percent / N,N-diisopropylethylamine / CH₂Cl₂ / 4 h

2: 97 percent / NaBH₄ / aq. ethanol

3: 98 percent / imidazole / dimethylformamide

With 1H-imidazole; sodium tetrahydroborate; N-ethyl-N,N-diisopropylamine; In ethanol; dichloromethane; N,N-dimethyl-formamide;