[(C₃H₅)Pd(O(C₂H₅)2)P(C₆H₁₁)3]⁽¹⁺⁾*[(C₆H₃(CF₃)2)4B]^(1-) = [(C₃H₅)Pd(O(C₂H₅)2)P(C₆H₁₁)3][(C₆H₃(CF₃)2)4B]

Base Information

• Chemical Name: [(C₃H₅)Pd(O(C₂H₅)2)P(C₆H₁₁)3]⁽¹⁺⁾*[(C₆H₃(CF₃)2)4B]^(1-) = [(C₃H₅)Pd(O(C₂H₅)2)P(C₆H₁₁)3][(C₆H₃(CF₃)2)4B]
• CAS No.: 179803-34-0
• Molecular Formula: C₂₅H₄₈OPPd*C₃₂H₁₂BF₂₄
• Molecular Weight: 1365.27

Synonyms:[(C₃H₅)Pd(O(C₂H₅)2)P(C₆H₁₁)3]⁽¹⁺⁾*[(C₆H₃(CF₃)2)4B]^(1-) = [(C₃H₅)Pd(O(C₂H₅)2)P(C₆H₁₁)3][(C₆H₃(CF₃)2)4B]

Chemical Property of [(C₃H₅)Pd(O(C₂H₅)2)P(C₆H₁₁)3]⁽¹⁺⁾*[(C₆H₃(CF₃)2)4B]^(1-) = [(C₃H₅)Pd(O(C₂H₅)2)P(C₆H₁₁)3][(C₆H₃(CF₃)2)4B]

Chemical Property:

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Technology Process of [(C₃H₅)Pd(O(C₂H₅)2)P(C₆H₁₁)3]⁽¹⁺⁾*[(C₆H₃(CF₃)2)4B]^(1-) = [(C₃H₅)Pd(O(C₂H₅)2)P(C₆H₁₁)3][(C₆H₃(CF₃)2)4B]

There total 3 articles about [(C₃H₅)Pd(O(C₂H₅)2)P(C₆H₁₁)3]⁽¹⁺⁾*[(C₆H₃(CF₃)2)4B]^(1-) = [(C₃H₅)Pd(O(C₂H₅)2)P(C₆H₁₁)3][(C₆H₃(CF₃)2)4B] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

tetrakis[3,5-bis(trifluoromethyl)phenyl]boric acid bis(diethyl ether) complex + (η3-allyl)PdMe(PCy3) → [(C3H5)Pd(O(C2H5)2)P(C6H11)3](1+)*[(C6H3(CF3)2)4B](1-) = [(C3H5)Pd(O(C2H5)2)P(C6H11)3][(C6H3(CF3)2)4B] (179803-34-0)

Guidance literature:

In diethyl ether; (N2 or Ar); stirring (-78°C, 1 h); evapn. (vac.), washing (hexane); elem. anal.;

DOI:10.1021/ja9602354

Reference yield:

(η(3)-allyl)PdCl * tricyclohexylphosphine (125893-61-0) → [(C3H5)Pd(O(C2H5)2)P(C6H11)3](1+)*[(C6H3(CF3)2)4B](1-) = [(C3H5)Pd(O(C2H5)2)P(C6H11)3][(C6H3(CF3)2)4B] (179803-34-0)

Guidance literature:

Multi-step reaction with 2 steps

1: diethyl ether

2: diethyl ether

In diethyl ether;

DOI:10.1021/ja9602354

Reference yield:

tricyclohexylphosphine (2622-14-2) → [(C3H5)Pd(O(C2H5)2)P(C6H11)3](1+)*[(C6H3(CF3)2)4B](1-) = [(C3H5)Pd(O(C2H5)2)P(C6H11)3][(C6H3(CF3)2)4B] (179803-34-0)

Guidance literature:

Multi-step reaction with 3 steps

1: diethyl ether

2: diethyl ether

3: diethyl ether

In diethyl ether;

DOI:10.1021/ja9602354

upstream raw materials:

(η(3)-allyl)PdCl * tricyclohexylphosphine

tricyclohexylphosphine

Downstream raw materials:

[(H₃CO(O)CCH₂CH₂)Pd(P(C₆H₁₁)3)(O(C₂H₅)2)]⁽¹⁺⁾*[(C₆H₃(CF₃)2)4B]^(1-) = [C₂₆H₅₀O₃PPd][C₃₂H₁₂BF₂₄]

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