(S)-2-amino-5-(((R)-1-((carboxymethyl)amino)-3-((4-nitrobenzoyl)thio)-1-oxopropan-2-yl)amino)-5-oxopentanoic acid

Base Information

• Chemical Name: (S)-2-amino-5-(((R)-1-((carboxymethyl)amino)-3-((4-nitrobenzoyl)thio)-1-oxopropan-2-yl)amino)-5-oxopentanoic acid
• CAS No.: 352320-23-1
• Molecular Formula: C₁₇H₂₀N₄O₉S
• Molecular Weight: 456.433

Synonyms:(S)-2-amino-5-(((R)-1-((carboxymethyl)amino)-3-((4-nitrobenzoyl)thio)-1-oxopropan-2-yl)amino)-5-oxopentanoic acid

Chemical Property of (S)-2-amino-5-(((R)-1-((carboxymethyl)amino)-3-((4-nitrobenzoyl)thio)-1-oxopropan-2-yl)amino)-5-oxopentanoic acid

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Technology Process of (S)-2-amino-5-(((R)-1-((carboxymethyl)amino)-3-((4-nitrobenzoyl)thio)-1-oxopropan-2-yl)amino)-5-oxopentanoic acid

There total 1 articles about (S)-2-amino-5-(((R)-1-((carboxymethyl)amino)-3-((4-nitrobenzoyl)thio)-1-oxopropan-2-yl)amino)-5-oxopentanoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

GLUTATHIONE (70-18-8) + 1H-1,2,3-benzotriazol-1-yl-4-nitrophenylmethanone (4231-71-4) → (S)-2-amino-5-(((R)-1-((carboxymethyl)amino)-3-((4-nitrobenzoyl)thio)-1-oxopropan-2-yl)amino)-5-oxopentanoic acid (352320-23-1)

Guidance literature:

With potassium hydrogencarbonate; In methanol; water; at 20 ℃;

DOI:10.1055/s-0029-1219837

Reference yield: 89.0%

N-Cbz-L-Leu-Bt + (S)-2-amino-5-(((R)-1-((carboxymethyl)amino)-3-((4-nitrobenzoyl)thio)-1-oxopropan-2-yl)amino)-5-oxopentanoic acid (352320-23-1) → C31H37N5O12S (1240115-72-3)

Guidance literature:

With triethylamine; In water; acetonitrile; at 20 ℃; for 1.5h;

DOI:10.1055/s-0029-1219837

Reference yield: 84.0%

(S)-2-amino-5-(((R)-1-((carboxymethyl)amino)-3-((4-nitrobenzoyl)thio)-1-oxopropan-2-yl)amino)-5-oxopentanoic acid (352320-23-1) + benzyl N-[(1S)-2-(1H-1,2,3-benzotriazol-1-yl)-1-methyl-2-oxoethyl]carbamate (820239-42-7) → (5S,8S,13R)-8-carboxy-5-methyl-13-(((4-nitrobenzoyl)thio)methyl)-3,6,11,14-tetraoxo-1-phenyl-2-oxa-4,7,12,15-tetraazaheptadecan-17-oic acid (1240115-69-8)

Guidance literature:

With triethylamine; In water; acetonitrile; at 20 ℃; for 1.5h;

DOI:10.1055/s-0029-1219837

upstream raw materials:

GLUTATHIONE

1H-1,2,3-benzotriazol-1-yl-4-nitrophenylmethanone

Downstream raw materials:

C₃₁H₃₇N₅O₁₂S

(5S,8S,13R)-8-carboxy-5-methyl-13-(((4-nitrobenzoyl)thio)methyl)-3,6,11,14-tetraoxo-1-phenyl-2-oxa-4,7,12,15-tetraazaheptadecan-17-oic acid

(5S,8S,13R)-5-benzyl-8-carboxy-13-(((4-nitrobenzoyl)thio)methyl)-3,6,11,14-tetraoxo-1-phenyl-2-oxa-4,7,12,15-tetraazaheptadecan-17-oic acid

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