5α,8α-(3,5-dioxo-4-phenyl-1,2,4-triazolidine-1,2-diyl)-9α,11α-epoxycholest-6-en-3β-yl acetate

Base Information

Chemical Name:5α,8α-(3,5-dioxo-4-phenyl-1,2,4-triazolidine-1,2-diyl)-9α,11α-epoxycholest-6-en-3β-yl acetate
CAS No.:89321-93-7
Molecular Formula:C₃₇H₄₉N₃O₅
Molecular Weight:615.813
Hs Code.:

Synonyms:5α,8α-(3,5-dioxo-4-phenyl-1,2,4-triazolidine-1,2-diyl)-9α,11α-epoxycholest-6-en-3β-yl acetate

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Chemical Property of 5α,8α-(3,5-dioxo-4-phenyl-1,2,4-triazolidine-1,2-diyl)-9α,11α-epoxycholest-6-en-3β-yl acetate

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Technology Process of 5α,8α-(3,5-dioxo-4-phenyl-1,2,4-triazolidine-1,2-diyl)-9α,11α-epoxycholest-6-en-3β-yl acetate

There total 3 articles about 5α,8α-(3,5-dioxo-4-phenyl-1,2,4-triazolidine-1,2-diyl)-9α,11α-epoxycholest-6-en-3β-yl acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: 89321-92-6
5α,8α-(3,5-dioxo-4-phenyl-1,2,4-triazolidine-1,2-diyl)cholesta-6,9(11)dien-3β-yl acetate

: 89321-93-7
5α,8α-(3,5-dioxo-4-phenyl-1,2,4-triazolidine-1,2-diyl)-9α,11α-epoxycholest-6-en-3β-yl acetate

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at 20 ℃; for 72h;
DOI:10.1002/ejoc.200400117

Reference yield:

: 1059-86-5
7-Dehydrocholesteryl acetate

: 89321-93-7
5α,8α-(3,5-dioxo-4-phenyl-1,2,4-triazolidine-1,2-diyl)-9α,11α-epoxycholest-6-en-3β-yl acetate

Guidance literature:: Multi-step reaction with 3 steps

1: 50 percent / mercuric acetate; acetic acid / ethanol / 0.5 h / Heating

2: 75 percent / acetone; CH₂Cl₂ / 0.25 h / -10 °C

3: 50 percent / m-chloroperbenzoic acid / CH₂Cl₂ / 72 h / 20 °C

With mercury(II) diacetate; acetic acid; 3-chloro-benzenecarboperoxoic acid; In ethanol; dichloromethane; acetone;
DOI:10.1002/ejoc.200400117

Reference yield:

: 1255-91-0
Δ^5,7,9-cholestatrien-3β-ol acetate

: 89321-93-7
5α,8α-(3,5-dioxo-4-phenyl-1,2,4-triazolidine-1,2-diyl)-9α,11α-epoxycholest-6-en-3β-yl acetate

Guidance literature:: Multi-step reaction with 2 steps

1: 75 percent / acetone; CH₂Cl₂ / 0.25 h / -10 °C

2: 50 percent / m-chloroperbenzoic acid / CH₂Cl₂ / 72 h / 20 °C

With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; acetone;
DOI:10.1002/ejoc.200400117