rel-(1S,2S,4R,11R,12R)-7-chloro-6-chloromethyl-8-oxo-4-phenyl-9-aza-3,5-dioxatetracyclo<10.2.1.0^2,11.0^4,9>pentadec-6-ene

Base Information

• Chemical Name: rel-(1S,2S,4R,11R,12R)-7-chloro-6-chloromethyl-8-oxo-4-phenyl-9-aza-3,5-dioxatetracyclo<10.2.1.0^2,11.0^4,9>pentadec-6-ene
• CAS No.: 100460-95-5
• Molecular Formula: C₁₉H₁₉Cl₂NO₃
• Molecular Weight: 380.271

Synonyms:rel-(1S,2S,4R,11R,12R)-7-chloro-6-chloromethyl-8-oxo-4-phenyl-9-aza-3,5-dioxatetracyclo<10.2.1.0^2,11.0^4,9>pentadec-6-ene

Chemical Property of rel-(1S,2S,4R,11R,12R)-7-chloro-6-chloromethyl-8-oxo-4-phenyl-9-aza-3,5-dioxatetracyclo<10.2.1.0^2,11.0^4,9>pentadec-6-ene

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Technology Process of rel-(1S,2S,4R,11R,12R)-7-chloro-6-chloromethyl-8-oxo-4-phenyl-9-aza-3,5-dioxatetracyclo<10.2.1.0^2,11.0^4,9>pentadec-6-ene

There total 1 articles about rel-(1S,2S,4R,11R,12R)-7-chloro-6-chloromethyl-8-oxo-4-phenyl-9-aza-3,5-dioxatetracyclo<10.2.1.0^2,11.0^4,9>pentadec-6-ene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 26.0%

r-4a,c-5,6,7,c-8,c-8a-Hexahydro-2-phenyl-5,8-methano-4H-1,3-benzoxazin (29266-28-2,120537-97-5) + chloroacetyl chloride (79-04-9) → rel-(1R,2S,4S,5R,9R,10S)-5-chloro-4-phenyl-6-oxo-7-aza-3-oxatetracyclo<8.2.1.02,9.04,7>tridecane (100460-89-7,120577-21-1) + rel-(1S,2S,4R,11R,12R)-7-chloro-6-chloromethyl-8-oxo-4-phenyl-9-aza-3,5-dioxatetracyclo<10.2.1.02,11.04,9>pentadec-6-ene (100460-95-5)

Guidance literature:

With TEA; In benzene; at 50 ℃; for 0.166667h;

DOI:10.1016/S0040-4020(01)96486-5

upstream raw materials:

r-4a,c-5,6,7,c-8,c-8a-Hexahydro-2-phenyl-5,8-methano-4H-1,3-benzoxazin

chloroacetyl chloride

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