2,2'-((4-methoxyphenylazanediyl)bis(2-methyl-5,1-phenylene))diisoindoline-1,3-dione

Base Information

Chemical Name:2,2'-((4-methoxyphenylazanediyl)bis(2-methyl-5,1-phenylene))diisoindoline-1,3-dione
CAS No.:1361344-10-6
Molecular Formula:C₃₇H₂₇N₃O₅
Molecular Weight:593.638
Hs Code.:

Synonyms:2,2'-((4-methoxyphenylazanediyl)bis(2-methyl-5,1-phenylene))diisoindoline-1,3-dione

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Chemical Property of 2,2'-((4-methoxyphenylazanediyl)bis(2-methyl-5,1-phenylene))diisoindoline-1,3-dione

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Technology Process of 2,2'-((4-methoxyphenylazanediyl)bis(2-methyl-5,1-phenylene))diisoindoline-1,3-dione

There total 3 articles about 2,2'-((4-methoxyphenylazanediyl)bis(2-methyl-5,1-phenylene))diisoindoline-1,3-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 85-44-9
phthalic anhydride

: 1361344-09-3
C₃₁H₃₉N₃O₅

: 1361344-10-6
2,2'-((4-methoxyphenylazanediyl)bis(2-methyl-5,1-phenylene))diisoindoline-1,3-dione

Guidance literature:: With acetic acid; at 119 ℃; for 4h; Inert atmosphere;
DOI:10.1016/j.tetlet.2011.12.028

Reference yield:

: 1361344-08-2
N-tert-butoxycarbonyl-5-iodo-2-methylaniline

: 1361344-10-6
2,2'-((4-methoxyphenylazanediyl)bis(2-methyl-5,1-phenylene))diisoindoline-1,3-dione

Guidance literature:: Multi-step reaction with 2 steps

1: [2,2]bipyridinyl; copper(l) iodide; potassium tert-butylate / toluene / 4 h / 120 °C / Inert atmosphere

2: acetic acid / 4 h / 119 °C / Inert atmosphere

With [2,2]bipyridinyl; copper(l) iodide; potassium tert-butylate; acetic acid; In toluene; 1: Ullmann condensation;
DOI:10.1016/j.tetlet.2011.12.028

Reference yield:

: 83863-33-6
5-iodo-o-toluidine

: 1361344-10-6
2,2'-((4-methoxyphenylazanediyl)bis(2-methyl-5,1-phenylene))diisoindoline-1,3-dione

Guidance literature:: Multi-step reaction with 3 steps

1: tetrahydrofuran / 2 h / Reflux; Inert atmosphere

2: [2,2]bipyridinyl; copper(l) iodide; potassium tert-butylate / toluene / 4 h / 120 °C / Inert atmosphere

3: acetic acid / 4 h / 119 °C / Inert atmosphere

With [2,2]bipyridinyl; copper(l) iodide; potassium tert-butylate; acetic acid; In tetrahydrofuran; toluene; 2: Ullmann condensation;
DOI:10.1016/j.tetlet.2011.12.028