(E)-2-[4,6-Bis-(4-methoxy-phenyl)-1,4,5,6-tetrahydro-[1,3,5]triazin-2-ylsulfanyl]-1-phenyl-ethenol

Base Information

• Chemical Name: (E)-2-[4,6-Bis-(4-methoxy-phenyl)-1,4,5,6-tetrahydro-[1,3,5]triazin-2-ylsulfanyl]-1-phenyl-ethenol
• CAS No.: 87102-25-8
• Molecular Formula: C₂₅H₂₅N₃O₃S
• Molecular Weight: 447.558

Synonyms:(E)-2-[4,6-Bis-(4-methoxy-phenyl)-1,4,5,6-tetrahydro-[1,3,5]triazin-2-ylsulfanyl]-1-phenyl-ethenol

Chemical Property of (E)-2-[4,6-Bis-(4-methoxy-phenyl)-1,4,5,6-tetrahydro-[1,3,5]triazin-2-ylsulfanyl]-1-phenyl-ethenol

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Technology Process of (E)-2-[4,6-Bis-(4-methoxy-phenyl)-1,4,5,6-tetrahydro-[1,3,5]triazin-2-ylsulfanyl]-1-phenyl-ethenol

There total 1 articles about (E)-2-[4,6-Bis-(4-methoxy-phenyl)-1,4,5,6-tetrahydro-[1,3,5]triazin-2-ylsulfanyl]-1-phenyl-ethenol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

α-bromoacetophenone (70-11-1) + 4,6-di(4-methoxyphenyl)[1,3,5]triazinane-2-thione (61582-11-4) → (E)-2-[4,6-Bis-(4-methoxy-phenyl)-1,4,5,6-tetrahydro-[1,3,5]triazin-2-ylsulfanyl]-1-phenyl-ethenol (87102-25-8)

Guidance literature:

With sodium hydroxide; In ethanol; for 2h; Heating;

DOI:10.1021/je00035a032

Reference yield: 78.0%

(E)-2-[4,6-Bis-(4-methoxy-phenyl)-1,4,5,6-tetrahydro-[1,3,5]triazin-2-ylsulfanyl]-1-phenyl-ethenol (87102-25-8) → 2,4-Bis-(4-methoxy-phenyl)-6-phenyl-3,4-dihydro-2H-thiazolo[3,2-a][1,3,5]triazine (87102-34-9)

Guidance literature:

With PPA; 1.) 100 deg C, 1 h, 2.) 120 deg C, 15 min;

DOI:10.1021/je00035a032

upstream raw materials:

α-bromoacetophenone

4,6-di(4-methoxyphenyl)[1,3,5]triazinane-2-thione

Downstream raw materials:

2,4-Bis-(4-methoxy-phenyl)-6-phenyl-3,4-dihydro-2H-thiazolo[3,2-a][1,3,5]triazine

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