(+)-(3R)-3-{[(4-methylphenyl)sulfonyl]amino}-N-{3-[[(4-methylphenyl)sulfonyl](4-{[(4-methylphenyl)sulfonyl]amino}butyl)amino]propyl}tetradecanamide

Base Information

Chemical Name:(+)-(3R)-3-{[(4-methylphenyl)sulfonyl]amino}-N-{3-[[(4-methylphenyl)sulfonyl](4-{[(4-methylphenyl)sulfonyl]amino}butyl)amino]propyl}tetradecanamide
CAS No.:467457-36-9
Molecular Formula:C₄₂H₆₄N₄O₇S₃
Molecular Weight:833.191
Hs Code.:

Synonyms:(+)-(3R)-3-{[(4-methylphenyl)sulfonyl]amino}-N-{3-[[(4-methylphenyl)sulfonyl](4-{[(4-methylphenyl)sulfonyl]amino}butyl)amino]propyl}tetradecanamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (+)-(3R)-3-{[(4-methylphenyl)sulfonyl]amino}-N-{3-[[(4-methylphenyl)sulfonyl](4-{[(4-methylphenyl)sulfonyl]amino}butyl)amino]propyl}tetradecanamide

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Technology Process of (+)-(3R)-3-{[(4-methylphenyl)sulfonyl]amino}-N-{3-[[(4-methylphenyl)sulfonyl](4-{[(4-methylphenyl)sulfonyl]amino}butyl)amino]propyl}tetradecanamide

There total 6 articles about (+)-(3R)-3-{[(4-methylphenyl)sulfonyl]amino}-N-{3-[[(4-methylphenyl)sulfonyl](4-{[(4-methylphenyl)sulfonyl]amino}butyl)amino]propyl}tetradecanamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 91652-58-3
N-(3-aminopropyl)-4-methyl-N-(4-{[(4-methylphenyl)sulfonyl]amino}butyl)benzenesulfonamide

: 467457-38-1
(+)-(3R)-3-{[(4-methylphenyl)sulfonyl]amino}tetradecanoic acid

: 467457-36-9
(+)-(3R)-3-{[(4-methylphenyl)sulfonyl]amino}-N-{3-[[(4-methylphenyl)sulfonyl](4-{[(4-methylphenyl)sulfonyl]amino}butyl)amino]propyl}tetradecanamide

Guidance literature:: With dmap; dicyclohexyl-carbodiimide; In dichloromethane; at 5 - 20 ℃;
DOI:10.1002/1522-2675(200206)85:6<1742::AID-HLCA1742>3.0.CO;2-E

Reference yield:

: 2050-77-3
Iododecane

: 467457-36-9
(+)-(3R)-3-{[(4-methylphenyl)sulfonyl]amino}-N-{3-[[(4-methylphenyl)sulfonyl](4-{[(4-methylphenyl)sulfonyl]amino}butyl)amino]propyl}tetradecanamide

Guidance literature:: Multi-step reaction with 3 steps

1.1: tBuLi / diethyl ether / 2 h / -78 - 20 °C

1.2: CuBr*Me₂S / tetrahydrofuran; diethyl ether / 0.5 h / -78 - 20 °C

1.3: 75 percent / tetrahydrofuran; diethyl ether / -78 - 20 °C

2.1: 98 percent / NaOH / ethanol; H₂O / 20 °C

3.1: 94 percent / DCC; DMAP / CH₂Cl₂ / 5 - 20 °C

With dmap; sodium hydroxide; tert.-butyl lithium; dicyclohexyl-carbodiimide; In diethyl ether; ethanol; dichloromethane; water;
DOI:10.1002/1522-2675(200206)85:6<1742::AID-HLCA1742>3.0.CO;2-E

Reference yield:

: 4748-73-6
N-(cyanoethyl)-1,4-diaminobutane

: 467457-36-9
(+)-(3R)-3-{[(4-methylphenyl)sulfonyl]amino}-N-{3-[[(4-methylphenyl)sulfonyl](4-{[(4-methylphenyl)sulfonyl]amino}butyl)amino]propyl}tetradecanamide

Guidance literature:: Multi-step reaction with 3 steps

1: 99 percent / Et₃N / tetrahydrofuran / 20 °C

2: 98 percent / NaBH₄; CF₃COOH / tetrahydrofuran / 2 h / 20 °C

3: 94 percent / DCC; DMAP / CH₂Cl₂ / 5 - 20 °C

With dmap; sodium tetrahydroborate; triethylamine; dicyclohexyl-carbodiimide; trifluoroacetic acid; In tetrahydrofuran; dichloromethane;
DOI:10.1002/1522-2675(200206)85:6<1742::AID-HLCA1742>3.0.CO;2-E