Technology Process of C13H11FO2S
There total 2 articles about C13H11FO2S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 3 steps
1: acetic acid; pyridinium hydrobromide perbromide; hydrogen bromide / 24 h / 20 °C
2: sulfuric acid / 24 h / Reflux
3: sodium carbonate; tetrakis(triphenylphosphine) palladium(0) / toluene; ethanol; water / 24 h / Reflux; Inert atmosphere
With
tetrakis(triphenylphosphine) palladium(0); pyridinium hydrobromide perbromide; sulfuric acid; hydrogen bromide; sodium carbonate; acetic acid;
In
ethanol; water; toluene;
DOI:10.1016/j.bioorg.2022.105704
- Guidance literature:
-
Multi-step reaction with 2 steps
1: sulfuric acid / 24 h / Reflux
2: sodium carbonate; tetrakis(triphenylphosphine) palladium(0) / toluene; ethanol; water / 24 h / Reflux; Inert atmosphere
With
tetrakis(triphenylphosphine) palladium(0); sulfuric acid; sodium carbonate;
In
ethanol; water; toluene;
DOI:10.1016/j.bioorg.2022.105704
- Guidance literature:
-
With
lithium diisopropyl amide;
In
tetrahydrofuran;
at 0 ℃;
for 0.5h;