N-(2-(1,3-dihydroxypropan-2-ylidene)nonyl)-N-methyl-2-nitrobenzenesulfonamide

Base Information

Chemical Name:N-(2-(1,3-dihydroxypropan-2-ylidene)nonyl)-N-methyl-2-nitrobenzenesulfonamide
CAS No.:1442642-89-8
Molecular Formula:C₁₉H₃₀N₂O₆S
Molecular Weight:414.523
Hs Code.:

Synonyms:N-(2-(1,3-dihydroxypropan-2-ylidene)nonyl)-N-methyl-2-nitrobenzenesulfonamide

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Chemical Property of N-(2-(1,3-dihydroxypropan-2-ylidene)nonyl)-N-methyl-2-nitrobenzenesulfonamide

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Technology Process of N-(2-(1,3-dihydroxypropan-2-ylidene)nonyl)-N-methyl-2-nitrobenzenesulfonamide

There total 5 articles about N-(2-(1,3-dihydroxypropan-2-ylidene)nonyl)-N-methyl-2-nitrobenzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 1442642-69-4
(E)-2-(hydroxymethyl)-3-((2-nitrophenylsulfonamido)methyl)dec-2-enyl acetate

: 74-88-4
methyl iodide

: 1442642-89-8
N-(2-(1,3-dihydroxypropan-2-ylidene)nonyl)-N-methyl-2-nitrobenzenesulfonamide

Guidance literature:: With potassium carbonate; In acetone; at 20 ℃; for 3h;
DOI:10.1002/adsc.201200242

Reference yield:

: C₁₅H₂₈O₃

: 1442642-89-8
N-(2-(1,3-dihydroxypropan-2-ylidene)nonyl)-N-methyl-2-nitrobenzenesulfonamide

Guidance literature:: Multi-step reaction with 4 steps

1: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / 0.5 h

2: toluene-4-sulfonic acid / methanol / 24 h

3: 2,4,6-trimethyl-pyridine; (2S,5S)-2,5-bis[[(2S)-3-(2-naphthylmethyl)-1-(octyloxy)-1-oxopropan-2-ylamino]carbonyl]-1-(pyridin-4-yl)pyrrolidine / chloroform / 24 h / -60 °C

4: potassium carbonate / acetone / 3 h / 20 °C

With 2,4,6-trimethyl-pyridine; (2S,5S)-2,5-bis[[(2S)-3-(2-naphthylmethyl)-1-(octyloxy)-1-oxopropan-2-ylamino]carbonyl]-1-(pyridin-4-yl)pyrrolidine; di-isopropyl azodicarboxylate; potassium carbonate; toluene-4-sulfonic acid; triphenylphosphine; In tetrahydrofuran; methanol; chloroform; acetone;
DOI:10.1002/adsc.201200242

Reference yield:

: 34066-51-8
Ethyl 2-(diethoxyphosphinyl)-nonanoate

: 1442642-89-8
N-(2-(1,3-dihydroxypropan-2-ylidene)nonyl)-N-methyl-2-nitrobenzenesulfonamide

Guidance literature:: Multi-step reaction with 6 steps

1.1: sodium hydride / tetrahydrofuran / 0.5 h / Reflux

1.2: 1 h / Reflux

2.1: diisobutylaluminium hydride / dichloromethane; toluene / 1 h / -30 °C

3.1: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / 0.5 h

4.1: toluene-4-sulfonic acid / methanol / 24 h

5.1: 2,4,6-trimethyl-pyridine; (2S,5S)-2,5-bis[[(2S)-3-(2-naphthylmethyl)-1-(octyloxy)-1-oxopropan-2-ylamino]carbonyl]-1-(pyridin-4-yl)pyrrolidine / chloroform / 24 h / -60 °C

6.1: potassium carbonate / acetone / 3 h / 20 °C

With 2,4,6-trimethyl-pyridine; (2S,5S)-2,5-bis[[(2S)-3-(2-naphthylmethyl)-1-(octyloxy)-1-oxopropan-2-ylamino]carbonyl]-1-(pyridin-4-yl)pyrrolidine; di-isopropyl azodicarboxylate; sodium hydride; diisobutylaluminium hydride; potassium carbonate; toluene-4-sulfonic acid; triphenylphosphine; In tetrahydrofuran; methanol; dichloromethane; chloroform; acetone; toluene;
DOI:10.1002/adsc.201200242