2-(4-(3-(4-(3,3-dimethyl-2-oxobutoxy)-3-methylphenyl)pentan-3-yl)-2-methylphenoxy)-N-hydroxyacetamide

Base Information

Chemical Name:2-(4-(3-(4-(3,3-dimethyl-2-oxobutoxy)-3-methylphenyl)pentan-3-yl)-2-methylphenoxy)-N-hydroxyacetamide
CAS No.:1416802-57-7
Molecular Formula:C₂₇H₃₇NO₅
Molecular Weight:455.594
Hs Code.:

Synonyms:2-(4-(3-(4-(3,3-dimethyl-2-oxobutoxy)-3-methylphenyl)pentan-3-yl)-2-methylphenoxy)-N-hydroxyacetamide

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Chemical Property of 2-(4-(3-(4-(3,3-dimethyl-2-oxobutoxy)-3-methylphenyl)pentan-3-yl)-2-methylphenoxy)-N-hydroxyacetamide

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Technology Process of 2-(4-(3-(4-(3,3-dimethyl-2-oxobutoxy)-3-methylphenyl)pentan-3-yl)-2-methylphenoxy)-N-hydroxyacetamide

There total 5 articles about 2-(4-(3-(4-(3,3-dimethyl-2-oxobutoxy)-3-methylphenyl)pentan-3-yl)-2-methylphenoxy)-N-hydroxyacetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 1416802-56-6
N-(benzyloxy)-2-(4-(3-(4-(3,3-dimethyl-2-oxobutoxy)-3-methylphenyl)pentan-3-yl)-2-methylphenoxy)acetamide

: 1416802-57-7
2-(4-(3-(4-(3,3-dimethyl-2-oxobutoxy)-3-methylphenyl)pentan-3-yl)-2-methylphenoxy)-N-hydroxyacetamide

Guidance literature:: With palladium 10% on activated carbon; hydrogen; In ethyl acetate; for 0.5h;

Reference yield:

: 55041-27-5
3,3-bis[4-hydroxy-3-methylphenyl]pentane

: 1416802-57-7
2-(4-(3-(4-(3,3-dimethyl-2-oxobutoxy)-3-methylphenyl)pentan-3-yl)-2-methylphenoxy)-N-hydroxyacetamide

Guidance literature:: Multi-step reaction with 5 steps

1.1: sodium hydride / N,N-dimethyl-formamide; paraffin oil / 2 h / 20 °C / Inert atmosphere

1.2: 16 h / Inert atmosphere

2.1: sodium hydride / N,N-dimethyl-formamide / 1 h / 0 - 20 °C / Inert atmosphere

2.2: 6 h / 80 °C / Inert atmosphere

3.1: lithium hydroxide monohydrate / tetrahydrofuran; water / 2 h / Inert atmosphere

4.1: N-ethyl-N,N-diisopropylamine; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate / N,N-dimethyl-formamide / 2 h / Inert atmosphere

5.1: palladium 10% on activated carbon; hydrogen / ethyl acetate / 0.5 h

With lithium hydroxide monohydrate; palladium 10% on activated carbon; hydrogen; sodium hydride; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; water; ethyl acetate; N,N-dimethyl-formamide; paraffin oil;

Reference yield:

: 1416802-51-1
ethyl 2-(4-(3-(4-hydroxy-3-methylphenyl)pentan-3-yl)-2-methylphenoxy)acetate

: 1416802-57-7
2-(4-(3-(4-(3,3-dimethyl-2-oxobutoxy)-3-methylphenyl)pentan-3-yl)-2-methylphenoxy)-N-hydroxyacetamide

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium hydride / N,N-dimethyl-formamide / 1 h / 0 - 20 °C / Inert atmosphere

1.2: 6 h / 80 °C / Inert atmosphere

2.1: lithium hydroxide monohydrate / tetrahydrofuran; water / 2 h / Inert atmosphere

3.1: N-ethyl-N,N-diisopropylamine; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate / N,N-dimethyl-formamide / 2 h / Inert atmosphere

4.1: palladium 10% on activated carbon; hydrogen / ethyl acetate / 0.5 h

With lithium hydroxide monohydrate; palladium 10% on activated carbon; hydrogen; sodium hydride; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; water; ethyl acetate; N,N-dimethyl-formamide;