ethyl 2-(4-(3-(4-hydroxy-3-methylphenyl)pentan-3-yl)-2-methylphenoxy)acetate

Base Information

Chemical Name:ethyl 2-(4-(3-(4-hydroxy-3-methylphenyl)pentan-3-yl)-2-methylphenoxy)acetate
CAS No.:1416802-51-1
Molecular Formula:C₂₃H₃₀O₄
Molecular Weight:370.489
Hs Code.:

Synonyms:ethyl 2-(4-(3-(4-hydroxy-3-methylphenyl)pentan-3-yl)-2-methylphenoxy)acetate

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Chemical Property of ethyl 2-(4-(3-(4-hydroxy-3-methylphenyl)pentan-3-yl)-2-methylphenoxy)acetate

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Technology Process of ethyl 2-(4-(3-(4-hydroxy-3-methylphenyl)pentan-3-yl)-2-methylphenoxy)acetate

There total 1 articles about ethyl 2-(4-(3-(4-hydroxy-3-methylphenyl)pentan-3-yl)-2-methylphenoxy)acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 35.0%

: 55041-27-5
3,3-bis[4-hydroxy-3-methylphenyl]pentane

: 105-36-2
ethyl bromoacetate

: 1416802-51-1
ethyl 2-(4-(3-(4-hydroxy-3-methylphenyl)pentan-3-yl)-2-methylphenoxy)acetate

: 1416802-52-2
diethyl 2,2-((pentane-3,3-diylbis(2-methyl-4,1-phenylene))bis(oxy))diacetate

Guidance literature:: 3,3-bis[4-hydroxy-3-methylphenyl]pentane; With sodium hydride; In N,N-dimethyl-formamide; paraffin oil; at 20 ℃; for 2h; Inert atmosphere;

ethyl bromoacetate; In N,N-dimethyl-formamide; paraffin oil; for 16h; Inert atmosphere;

Reference yield: 43.0%

: 13547-70-1
1-chloro-3,3-dimethyl-butan-2-one

: 1416802-51-1
ethyl 2-(4-(3-(4-hydroxy-3-methylphenyl)pentan-3-yl)-2-methylphenoxy)acetate

: 1332724-93-2
(4-{1-[4-(3,3-dimethyl-2-oxobutoxy)-3-methylphenyl]-1-ethylpropyl}-2-methylphenoxy)-acetic acid ethyl ester

Guidance literature:: ethyl 2-(4-(3-(4-hydroxy-3-methylphenyl)pentan-3-yl)-2-methylphenoxy)acetate; With sodium hydride; In N,N-dimethyl-formamide; at 0 - 20 ℃; for 1h; Inert atmosphere;

1-chloro-3,3-dimethyl-butan-2-one; In N,N-dimethyl-formamide; at 80 ℃; for 6h; Inert atmosphere;

Reference yield:

: 1416802-51-1
ethyl 2-(4-(3-(4-hydroxy-3-methylphenyl)pentan-3-yl)-2-methylphenoxy)acetate

: 1416802-59-9
ethyl 2-(4-(3-(4-((2R)-hydroxy-3,3-dimethylbutoxy)-3-methylphenyl)pentan-3-yl)-2-methylphenoxy)acetate

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydride / N,N-dimethyl-formamide / 1 h / 0 - 20 °C / Inert atmosphere

1.2: 6 h / 80 °C / Inert atmosphere

2.1: dimethylsulfide borane complex; (3aR)-1-methyl-3,3-diphenyl-tetrahydro-pyrrolo[1,2-c][1,3,2]oxazaborole / toluene / 0.17 h / 20 °C / Inert atmosphere

With dimethylsulfide borane complex; sodium hydride; (3aR)-1-methyl-3,3-diphenyl-tetrahydro-pyrrolo[1,2-c][1,3,2]oxazaborole; In N,N-dimethyl-formamide; toluene;