benzyl 4'-(2,4-dibenzyloxy-6-pentadecanylbenzoyloxy)-2'-hydroxy-6'-methylbenzoate

Base Information

Chemical Name:benzyl 4'-(2,4-dibenzyloxy-6-pentadecanylbenzoyloxy)-2'-hydroxy-6'-methylbenzoate
CAS No.:869996-10-1
Molecular Formula:C₅₁H₆₀O₇
Molecular Weight:785.033
Hs Code.:

Synonyms:benzyl 4'-(2,4-dibenzyloxy-6-pentadecanylbenzoyloxy)-2'-hydroxy-6'-methylbenzoate

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Chemical Property of benzyl 4'-(2,4-dibenzyloxy-6-pentadecanylbenzoyloxy)-2'-hydroxy-6'-methylbenzoate

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Technology Process of benzyl 4'-(2,4-dibenzyloxy-6-pentadecanylbenzoyloxy)-2'-hydroxy-6'-methylbenzoate

There total 10 articles about benzyl 4'-(2,4-dibenzyloxy-6-pentadecanylbenzoyloxy)-2'-hydroxy-6'-methylbenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 869996-09-8
2,4-bis(benzyloxy)-6-pentadecanylbenzoic acid

: 38862-71-4
benzyl 2,4-dihydroxy-6-methylbenzoate

: 869996-10-1
benzyl 4'-(2,4-dibenzyloxy-6-pentadecanylbenzoyloxy)-2'-hydroxy-6'-methylbenzoate

Guidance literature:: With trifluoroacetic anhydride; In toluene; at 20 ℃; for 2h;
DOI:10.1021/jo051384k

Reference yield:

: 869996-08-7
2,4-bis-benzyloxy-6-pentadecyl-benzoic acid ethyl ester

: 869996-10-1
benzyl 4'-(2,4-dibenzyloxy-6-pentadecanylbenzoyloxy)-2'-hydroxy-6'-methylbenzoate

Guidance literature:: Multi-step reaction with 2 steps

1: 1.40 g / KOH / dimethylsulfoxide; H₂O / 24 h / 90 °C

2: 94 percent / (CF₃CO)2O / toluene / 2 h / 20 °C

With potassium hydroxide; trifluoroacetic anhydride; In water; dimethyl sulfoxide; toluene;
DOI:10.1021/jo051384k

Reference yield:

: 504-15-4
orcinol

: 869996-10-1
benzyl 4'-(2,4-dibenzyloxy-6-pentadecanylbenzoyloxy)-2'-hydroxy-6'-methylbenzoate

Guidance literature:: Multi-step reaction with 4 steps

1.1: POCl₃ / 12 h / 20 °C

1.2: 80 percent / NaOH / H₂O / 0.17 h / pH 10 / Heating

2.1: 77 percent / NaH₂PO₄; NaClO₂ / H₂O; dimethylsulfoxide / 20 °C

3.1: 78 percent / KHCO₃ / dimethylformamide / 20 °C

4.1: 94 percent / (CF₃CO)2O / toluene / 2 h / 20 °C

With sodium chlorite; sodium dihydrogenphosphate; potassium hydrogencarbonate; trifluoroacetic anhydride; trichlorophosphate; In water; dimethyl sulfoxide; N,N-dimethyl-formamide; toluene;
DOI:10.1021/jo051384k