benzyl 4'-(2,4-dihydroxy-6-pentadecanylbenzoyloxy)-2'-hydroxy-6'-methylbenzoate

Base Information

Chemical Name:benzyl 4'-(2,4-dihydroxy-6-pentadecanylbenzoyloxy)-2'-hydroxy-6'-methylbenzoate
CAS No.:869996-11-2
Molecular Formula:C₃₇H₄₈O₇
Molecular Weight:604.784
Hs Code.:

Synonyms:benzyl 4'-(2,4-dihydroxy-6-pentadecanylbenzoyloxy)-2'-hydroxy-6'-methylbenzoate

Suppliers and Price of benzyl 4'-(2,4-dihydroxy-6-pentadecanylbenzoyloxy)-2'-hydroxy-6'-methylbenzoate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of benzyl 4'-(2,4-dihydroxy-6-pentadecanylbenzoyloxy)-2'-hydroxy-6'-methylbenzoate

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of benzyl 4'-(2,4-dihydroxy-6-pentadecanylbenzoyloxy)-2'-hydroxy-6'-methylbenzoate

There total 13 articles about benzyl 4'-(2,4-dihydroxy-6-pentadecanylbenzoyloxy)-2'-hydroxy-6'-methylbenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 160219-85-2
4'-(2,4-dihydroxy-6-pentadecanylbenzoyloxy)-2'-hydroxy-6'-methylbenzoic acid

: 100-39-0
benzyl bromide

: 869996-11-2
benzyl 4'-(2,4-dihydroxy-6-pentadecanylbenzoyloxy)-2'-hydroxy-6'-methylbenzoate

Guidance literature:: With potassium hydrogencarbonate; In N,N-dimethyl-formamide; at 20 ℃; for 40h;
DOI:10.1021/jo051384k

Reference yield:

: 869996-09-8
2,4-bis(benzyloxy)-6-pentadecanylbenzoic acid

: 869996-11-2
benzyl 4'-(2,4-dihydroxy-6-pentadecanylbenzoyloxy)-2'-hydroxy-6'-methylbenzoate

Guidance literature:: Multi-step reaction with 3 steps

1: 94 percent / (CF₃CO)2O / toluene / 2 h / 20 °C

2: 100 percent / H₂ / Pd/C / ethyl acetate / 96 h / 20 °C / 760 Torr

3: 89 percent / KHCO₃ / dimethylformamide / 40 h / 20 °C

With hydrogen; potassium hydrogencarbonate; trifluoroacetic anhydride; palladium on activated charcoal; In ethyl acetate; N,N-dimethyl-formamide; toluene;
DOI:10.1021/jo051384k

Reference yield:

: 869996-08-7
2,4-bis-benzyloxy-6-pentadecyl-benzoic acid ethyl ester

: 869996-11-2
benzyl 4'-(2,4-dihydroxy-6-pentadecanylbenzoyloxy)-2'-hydroxy-6'-methylbenzoate

Guidance literature:: Multi-step reaction with 4 steps

1: 1.40 g / KOH / dimethylsulfoxide; H₂O / 24 h / 90 °C

2: 94 percent / (CF₃CO)2O / toluene / 2 h / 20 °C

3: 100 percent / H₂ / Pd/C / ethyl acetate / 96 h / 20 °C / 760 Torr

4: 89 percent / KHCO₃ / dimethylformamide / 40 h / 20 °C

With potassium hydroxide; hydrogen; potassium hydrogencarbonate; trifluoroacetic anhydride; palladium on activated charcoal; In water; dimethyl sulfoxide; ethyl acetate; N,N-dimethyl-formamide; toluene;
DOI:10.1021/jo051384k