(Z)-2-(3-chlorobenzylidene)-3-oxo-2,3-dihydrobenzofuran-5-yl 10-undecylenate

Base Information

Chemical Name:(Z)-2-(3-chlorobenzylidene)-3-oxo-2,3-dihydrobenzofuran-5-yl 10-undecylenate
CAS No.:1311272-13-5
Molecular Formula:C₂₆H₂₇ClO₄
Molecular Weight:438.951
Hs Code.:

Synonyms:(Z)-2-(3-chlorobenzylidene)-3-oxo-2,3-dihydrobenzofuran-5-yl 10-undecylenate

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Chemical Property of (Z)-2-(3-chlorobenzylidene)-3-oxo-2,3-dihydrobenzofuran-5-yl 10-undecylenate

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Technology Process of (Z)-2-(3-chlorobenzylidene)-3-oxo-2,3-dihydrobenzofuran-5-yl 10-undecylenate

There total 6 articles about (Z)-2-(3-chlorobenzylidene)-3-oxo-2,3-dihydrobenzofuran-5-yl 10-undecylenate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 38460-95-6
undec-10-enoyl chloride

: 1234351-42-8
(Z)-2-(3-chlorobenzylidene)-5-hydroxybenzo[b]furan-3-one

: 1311272-13-5
(Z)-2-(3-chlorobenzylidene)-3-oxo-2,3-dihydrobenzofuran-5-yl 10-undecylenate

Guidance literature:: With pyridine; In dichloromethane; Reflux;
DOI:10.1016/j.bmc.2011.03.063

Reference yield:

: 112-38-9
10-undecenoic acid

: 1311272-13-5
(Z)-2-(3-chlorobenzylidene)-3-oxo-2,3-dihydrobenzofuran-5-yl 10-undecylenate

Guidance literature:: Multi-step reaction with 2 steps

1: phosphorus trichloride / 3 h / 70 °C

2: pyridine / dichloromethane / Reflux

With pyridine; phosphorus trichloride; In dichloromethane;
DOI:10.1016/j.bmc.2011.03.063

Reference yield:

: 1311272-38-4
2'-hydroxy-5'-(methoxymethoxy)-3-chlorochalcone

: 1311272-13-5
(Z)-2-(3-chlorobenzylidene)-3-oxo-2,3-dihydrobenzofuran-5-yl 10-undecylenate

Guidance literature:: Multi-step reaction with 3 steps

1: pyridine; mercury(II) diacetate / 1 h / 110 °C

2: hydrogenchloride; water / methanol / 0.5 h / Reflux

3: pyridine / dichloromethane / Reflux

With pyridine; hydrogenchloride; mercury(II) diacetate; water; In methanol; dichloromethane;
DOI:10.1016/j.bmc.2011.03.063