C₂₇H₃₅NO₂Si

Base Information

Chemical Name:C₂₇H₃₅NO₂Si
CAS No.:1603898-75-4
Molecular Formula:C₂₇H₃₅NO₂Si
Molecular Weight:433.666
Hs Code.:

C<sub>27</sub>H<sub>35</sub>NO<sub>2</sub>Si

Synonyms:C₂₇H₃₅NO₂Si

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Chemical Property of C₂₇H₃₅NO₂Si

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Technology Process of C₂₇H₃₅NO₂Si

There total 4 articles about C₂₇H₃₅NO₂Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 1603898-62-9
N,N-diethyl-O-([1-phenyl-3-(triethylsilyl)]naphth-2-yl)-carbamate

: 1603898-75-4
C₂₇H₃₅NO₂Si

Guidance literature:: With lithium diisopropyl amide; In tetrahydrofuran; for 18h; Microwave irradiation;
DOI:10.1021/ol500707w

Reference yield:

: 61912-14-9
2-naphthyl diethylcarbamate

: 1603898-75-4
C₂₇H₃₅NO₂Si

Guidance literature:: Multi-step reaction with 4 steps

1.1: 2,2,6,6-tetramethylpiperidinyl-lithium / tetrahydrofuran / 1.5 h / -78 °C / Inert atmosphere

1.2: 2 h / -78 - 20 °C / Inert atmosphere

2.1: tert.-butyl lithium / diethyl ether; pentane / 0.58 h / -78 °C

2.2: 0.5 h / -78 - 20 °C

3.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate / 1,2-dimethoxyethane / 19 h / Inert atmosphere; Reflux

4.1: lithium diisopropyl amide / tetrahydrofuran / 18 h / Microwave irradiation

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; 2,2,6,6-tetramethylpiperidinyl-lithium; tert.-butyl lithium; potassium carbonate; lithium diisopropyl amide; In tetrahydrofuran; 1,2-dimethoxyethane; diethyl ether; pentane; 3.1: |Suzuki-Miyaura Coupling;
DOI:10.1021/ol500707w

Reference yield:

: 1603898-34-5
N,N-diethyl-O-((1-iodo-3-(triethylsilyl))naphth-2-yl)-carbamate

: 1603898-75-4
C₂₇H₃₅NO₂Si

Guidance literature:: Multi-step reaction with 2 steps

1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate / 1,2-dimethoxyethane / 19 h / Inert atmosphere; Reflux

2: lithium diisopropyl amide / tetrahydrofuran / 18 h / Microwave irradiation

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate; lithium diisopropyl amide; In tetrahydrofuran; 1,2-dimethoxyethane; 1: |Suzuki-Miyaura Coupling;
DOI:10.1021/ol500707w