Technology Process of 1-(4-benzyloxy-3-tert-butylphenyl)ethanone
There total 5 articles about 1-(4-benzyloxy-3-tert-butylphenyl)ethanone which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
-butyl vinyl ether; 1-benzyloxy-4-bromo-2-tert-butylbenzene;
With
1,3-bis-(diphenylphosphino)propane; palladium diacetate; potassium carbonate;
In
water; N,N-dimethyl-formamide;
at 25 - 150 ℃;
for 5h;
Inert atmosphere;
With
hydrogenchloride;
In
water; N,N-dimethyl-formamide;
at 25 ℃;
for 2h;
Inert atmosphere;
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: sodium hydride / N,N-dimethyl-formamide / 0.17 h / 20 °C / Inert atmosphere
1.2: 2 h / 20 °C / Inert atmosphere
2.1: potassium carbonate; palladium diacetate; 1,3-bis-(diphenylphosphino)propane / N,N-dimethyl-formamide; water / 5 h / 25 - 150 °C / Inert atmosphere
2.2: 2 h / 25 °C / Inert atmosphere
With
1,3-bis-(diphenylphosphino)propane; palladium diacetate; sodium hydride; potassium carbonate;
In
water; N,N-dimethyl-formamide;
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: sodium hydride / N,N-dimethyl-formamide / 0.17 h / 20 °C / Inert atmosphere
1.2: 2 h / 20 °C / Inert atmosphere
2.1: potassium carbonate; palladium diacetate; 1,3-bis-(diphenylphosphino)propane / N,N-dimethyl-formamide; water / 5 h / 25 - 150 °C / Inert atmosphere
2.2: 2 h / 25 °C / Inert atmosphere
With
1,3-bis-(diphenylphosphino)propane; palladium diacetate; sodium hydride; potassium carbonate;
In
water; N,N-dimethyl-formamide;
