(S)-5-[4-(tert-Butyl-diphenyl-silanyloxy)-butyl]-5-methyl-tetrahydro-furan-2-ol

Base Information

• Chemical Name: (S)-5-[4-(tert-Butyl-diphenyl-silanyloxy)-butyl]-5-methyl-tetrahydro-furan-2-ol
• CAS No.: 123171-33-5
• Molecular Formula: C₂₅H₃₆O₃Si
• Molecular Weight: 412.645

Synonyms:(S)-5-[4-(tert-Butyl-diphenyl-silanyloxy)-butyl]-5-methyl-tetrahydro-furan-2-ol

Chemical Property of (S)-5-[4-(tert-Butyl-diphenyl-silanyloxy)-butyl]-5-methyl-tetrahydro-furan-2-ol

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Technology Process of (S)-5-[4-(tert-Butyl-diphenyl-silanyloxy)-butyl]-5-methyl-tetrahydro-furan-2-ol

There total 6 articles about (S)-5-[4-(tert-Butyl-diphenyl-silanyloxy)-butyl]-5-methyl-tetrahydro-furan-2-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

carbon monoxide (201230-82-2) + (S)-7-(tert-Butyl-diphenyl-silanyloxy)-3-methyl-hept-1-en-3-ol (123171-31-3) → (S)-5-[4-(tert-Butyl-diphenyl-silanyloxy)-butyl]-5-methyl-tetrahydro-furan-2-ol (123171-33-5)

Guidance literature:

With carbonylchlorohydridotris(triphenylphosphine)ruthenium(II); hydrogen; triethylamine; In benzene; under 37503 Torr;

Reference yield:

carbon monoxide (201230-82-2) + (S)-7-(tert-Butyl-diphenyl-silanyloxy)-3-methyl-hept-1-en-3-ol (123171-31-3) → (R)-5-[4-(tert-Butyl-diphenyl-silanyloxy)-butyl]-5-methyl-tetrahydro-furan-2-ol (123171-33-5) + (S)-5-[4-(tert-Butyl-diphenyl-silanyloxy)-butyl]-5-methyl-tetrahydro-furan-2-ol (123171-33-5)

Guidance literature:

With carbonylchlorohydridotris(triphenylphosphine)ruthenium(II); hydrogen; triethylamine; In benzene; under 37503 Torr;

Reference yield:

carbon monoxide (201230-82-2) + (S)-7-(tert-Butyl-diphenyl-silanyloxy)-3-methyl-hept-1-en-3-ol (123171-31-3) → (R)-5-[4-(tert-Butyl-diphenyl-silanyloxy)-butyl]-5-methyl-tetrahydro-furan-2-ol (123171-33-5) + (S)-5-[4-(tert-Butyl-diphenyl-silanyloxy)-butyl]-5-methyl-tetrahydro-furan-2-ol (123171-33-5)

Guidance literature:

With carbonylchlorohydridotris(triphenylphosphine)ruthenium(II); hydrogen; triethylamine; In benzene; under 37503 Torr;

upstream raw materials:

carbon monoxide

(S)-7-(tert-Butyl-diphenyl-silanyloxy)-3-methyl-hept-1-en-3-ol

6-(tert-butyldiphenylsilyloxy)hexan-2-one

Downstream raw materials:

tert-Butyl-[4-((S)-2-methyl-2,3-dihydro-furan-2-yl)-butoxy]-diphenyl-silane

tert-Butyl-[4-((R)-2-methyl-2,3-dihydro-furan-2-yl)-butoxy]-diphenyl-silane

tert-Butyl-[4-((S)-2-methyl-2,3-dihydro-furan-2-yl)-butoxy]-diphenyl-silane

C₂₅H₃₃LiO₂Si

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