1-iodo-8-[4'-(8''-[2''',5'''-dimethoxyphenyl]-1''-naphthyl)-1'-phenyl]naphthalene

Base Information

Chemical Name:1-iodo-8-[4'-(8''-[2''',5'''-dimethoxyphenyl]-1''-naphthyl)-1'-phenyl]naphthalene
CAS No.:303006-88-4
Molecular Formula:C₃₄H₂₅IO₂
Molecular Weight:592.476
Hs Code.:

Synonyms:1-iodo-8-[4'-(8''-[2''',5'''-dimethoxyphenyl]-1''-naphthyl)-1'-phenyl]naphthalene

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Chemical Property of 1-iodo-8-[4'-(8''-[2''',5'''-dimethoxyphenyl]-1''-naphthyl)-1'-phenyl]naphthalene

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Technology Process of 1-iodo-8-[4'-(8''-[2''',5'''-dimethoxyphenyl]-1''-naphthyl)-1'-phenyl]naphthalene

There total 6 articles about 1-iodo-8-[4'-(8''-[2''',5'''-dimethoxyphenyl]-1''-naphthyl)-1'-phenyl]naphthalene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 35.0%

: 1730-04-7
1,8-diiodonaphthalene

: 303006-87-3
1-(2,5-dimethoxyphenyl)-8-[4-(4',4',5',5'-tetramethyl[1',3',2']dioxaborolan-2'-yl)-1-phenyl]naphthalene

: 303006-88-4
1-iodo-8-[4'-(8''-[2''',5'''-dimethoxyphenyl]-1''-naphthyl)-1'-phenyl]naphthalene

Guidance literature:: With barium dihydroxide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In 1,2-dimethoxyethane; at 80 ℃; for 1h;
DOI:10.1021/ja000759a

Reference yield:

: 1730-04-7
1,8-diiodonaphthalene

: 303006-88-4
1-iodo-8-[4'-(8''-[2''',5'''-dimethoxyphenyl]-1''-naphthyl)-1'-phenyl]naphthalene

Guidance literature:: Multi-step reaction with 3 steps

1.1: ZnCl₂ / tetrahydrofuran / 0.25 h

1.2: 595 mg / Pd(PPh₃)4 / tetrahydrofuran / 12 h

2.1: 57 percent / Pd(PPh₃)4; K₃PO₄ / dimethylformamide / 2 h / 100 °C

3.1: 35 percent / aq. Ba(OH)2; Pd(PPh₃)4 / 1,2-dimethoxy-ethane / 1 h / 80 °C

With barium dihydroxide; potassium phosphate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; zinc(II) chloride; In tetrahydrofuran; 1,2-dimethoxyethane; N,N-dimethyl-formamide; 1.1: Metallation / 2.1: Condensation / 3.1: Condensation;
DOI:10.1021/ja000759a

Reference yield:

: 106-37-6
1.4-dibromobenzene

: 303006-88-4
1-iodo-8-[4'-(8''-[2''',5'''-dimethoxyphenyl]-1''-naphthyl)-1'-phenyl]naphthalene

Guidance literature:: Multi-step reaction with 3 steps

1: 31 percent / KOAc; PdCl₂(dppf) / dimethylformamide / 2 h / 80 °C

2: 57 percent / Pd(PPh₃)4; K₃PO₄ / dimethylformamide / 2 h / 100 °C

3: 35 percent / aq. Ba(OH)2; Pd(PPh₃)4 / 1,2-dimethoxy-ethane / 1 h / 80 °C

With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; barium dihydroxide; potassium phosphate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium acetate; In 1,2-dimethoxyethane; N,N-dimethyl-formamide; 1: Condensation / 2: Condensation / 3: Condensation;
DOI:10.1021/ja000759a