[5-[8'-(4''-[8'''-(2'''',5''''-dimethoxyphenyl)-1'''-naphthyl]-1''-phenyl)-1'-naphthyl]-10,20-diphenylporphinato]zinc(II)

Base Information

Chemical Name:[5-[8'-(4''-[8'''-(2'''',5''''-dimethoxyphenyl)-1'''-naphthyl]-1''-phenyl)-1'-naphthyl]-10,20-diphenylporphinato]zinc(II)
CAS No.:303052-58-6
Molecular Formula:C₆₆H₄₄N₄O₂Zn
Molecular Weight:990.491
Hs Code.:

Synonyms:[5-[8'-(4''-[8'''-(2'''',5''''-dimethoxyphenyl)-1'''-naphthyl]-1''-phenyl)-1'-naphthyl]-10,20-diphenylporphinato]zinc(II)

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Chemical Property of [5-[8'-(4''-[8'''-(2'''',5''''-dimethoxyphenyl)-1'''-naphthyl]-1''-phenyl)-1'-naphthyl]-10,20-diphenylporphinato]zinc(II)

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Technology Process of [5-[8'-(4''-[8'''-(2'''',5''''-dimethoxyphenyl)-1'''-naphthyl]-1''-phenyl)-1'-naphthyl]-10,20-diphenylporphinato]zinc(II)

There total 1 articles about [5-[8'-(4''-[8'''-(2'''',5''''-dimethoxyphenyl)-1'''-naphthyl]-1''-phenyl)-1'-naphthyl]-10,20-diphenylporphinato]zinc(II) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 219640-18-3
[5-(4',4',5',5'-tetramethyl[1',3',2']-dioxaborolan-2'-yl)-10,20-diphenylporphyrinato]zinc(II)

: 303006-88-4
1-iodo-8-[4'-(8''-[2''',5'''-dimethoxyphenyl]-1''-naphthyl)-1'-phenyl]naphthalene

: (5,15-diphenylporphinato)zinc(II)

: 303052-58-6
[5-[8'-(4''-[8'''-(2'''',5''''-dimethoxyphenyl)-1'''-naphthyl]-1''-phenyl)-1'-naphthyl]-10,20-diphenylporphinato]zinc(II)

Guidance literature:: With barium dihydroxide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In 1,2-dimethoxyethane; water; ligand, Zn-complex and Ba(OH)2*8H2O were dissolved in H2O and DME, Pd-complex was added, mixt. was heated at 80°C for 1 h under N2; benzene and satd. soln. of NaCl were added, organic layer was washed with NaCl and H2O, dried over CaCl2, filtered, evapd., chromy. on silica gel with hexane/THF;
DOI:10.1021/ja000759a