(1S,3R,5S)-1,7-bis(4-hydroxy-3-methoxyphenyl)-1,5-epoxy-3-hydroxyheptane

Base Information

Chemical Name:(1S,3R,5S)-1,7-bis(4-hydroxy-3-methoxyphenyl)-1,5-epoxy-3-hydroxyheptane
CAS No.:1443418-27-6
Molecular Formula:C₂₁H₂₆O₆
Molecular Weight:374.434
Hs Code.:

Synonyms:(1S,3R,5S)-1,7-bis(4-hydroxy-3-methoxyphenyl)-1,5-epoxy-3-hydroxyheptane

Suppliers and Price of (1S,3R,5S)-1,7-bis(4-hydroxy-3-methoxyphenyl)-1,5-epoxy-3-hydroxyheptane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (1S,3R,5S)-1,7-bis(4-hydroxy-3-methoxyphenyl)-1,5-epoxy-3-hydroxyheptane

Chemical Property:

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Technology Process of (1S,3R,5S)-1,7-bis(4-hydroxy-3-methoxyphenyl)-1,5-epoxy-3-hydroxyheptane

There total 10 articles about (1S,3R,5S)-1,7-bis(4-hydroxy-3-methoxyphenyl)-1,5-epoxy-3-hydroxyheptane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 1616883-94-3
C₂₈H₃₂O₆

: 1443418-27-6
(1S,3R,5S)-1,7-bis(4-hydroxy-3-methoxyphenyl)-1,5-epoxy-3-hydroxyheptane

Guidance literature:: With palladium hydroxide, 20 wt% on carbon; hydrogen; In tetrahydrofuran; at 25 ℃;
DOI:10.1016/j.tetlet.2014.04.065

Reference yield:

: dioscorosides E₁

: 1443418-27-6
(1S,3R,5S)-1,7-bis(4-hydroxy-3-methoxyphenyl)-1,5-epoxy-3-hydroxyheptane

Guidance literature:: With β-glucosidase; In water; at 37 ℃; for 12h; Enzymatic reaction;
DOI:10.1016/j.fitote.2017.01.004

Reference yield:

: 121-33-5,8014-42-4
vanillin

: 1443418-27-6
(1S,3R,5S)-1,7-bis(4-hydroxy-3-methoxyphenyl)-1,5-epoxy-3-hydroxyheptane

Guidance literature:: Multi-step reaction with 4 steps

1: triethylamine / dichloromethane / 0 - 25 °C

2: trifluoroacetic acid / dichloromethane / 16 h / 0 °C

3: potassium carbonate / methanol / 1 h / Reflux

4: palladium hydroxide, 20 wt% on carbon; hydrogen / tetrahydrofuran / 25 °C

With palladium hydroxide, 20 wt% on carbon; hydrogen; potassium carbonate; triethylamine; trifluoroacetic acid; In tetrahydrofuran; methanol; dichloromethane;
DOI:10.1016/j.tetlet.2014.04.065