C₄₀H₅₂N₆O₆S

Base Information

Chemical Name:C₄₀H₅₂N₆O₆S
CAS No.:271800-39-6
Molecular Formula:C₄₀H₅₂N₆O₆S
Molecular Weight:744.955
Hs Code.:

C<sub>40</sub>H<sub>52</sub>N<sub>6</sub>O<sub>6</sub>S

Synonyms:C₄₀H₅₂N₆O₆S

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Chemical Property of C₄₀H₅₂N₆O₆S

Chemical Property:

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Technology Process of C₄₀H₅₂N₆O₆S

There total 6 articles about C₄₀H₅₂N₆O₆S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 39021-83-5
3,6-dimethoxy-o-xylene

: 271800-39-6
C₄₀H₅₂N₆O₆S

Guidance literature:: Multi-step reaction with 7 steps

1.1: 61 percent / Nh₄NO₃; trifluoroacetic anhydride / acetonitrile / 2.5 h / 20 °C

2.1: 96 percent / H₂ / Ra-Ni / tetrahydrofuran / 18 h

3.1: SO₂NH₂ / bis-(2-methoxy-ethyl) ether / Heating

3.2: 41 percent / DMAP / 24 h / 20 °C

4.1: 100 percent / N-bromosuccinimide / CCl₄ / 1.5 h / Heating

5.1: KO-t-Bu

6.1: cerium ammonium nitrate

7.1: CF₃COOH / CH₂Cl₂ / 2 h / 20 °C

With ammonium nitrate; N-Bromosuccinimide; ammonium cerium(IV) nitrate; potassium tert-butylate; hydrogen; SULFAMIDE; trifluoroacetic acid; trifluoroacetic anhydride; Ra-Ni; In tetrahydrofuran; tetrachloromethane; dichloromethane; diethylene glycol dimethyl ether; acetonitrile; 1.1: Substitution / 2.1: Catalytic hydrogenation / 3.1: Cyclization / 3.2: Acylation / 4.1: Bromination / 5.1: Substitution / 5.2: Cyclization / 6.1: Oxidation / 7.1: Hydrolysis;
DOI:10.1021/ja0005136

Reference yield:

: 186039-76-9
1,4-dimethoxy-5,6-dimethyl-2,3-dinitrobenzene

: 271800-39-6
C₄₀H₅₂N₆O₆S

Guidance literature:: Multi-step reaction with 6 steps

1.1: 96 percent / H₂ / Ra-Ni / tetrahydrofuran / 18 h

2.1: SO₂NH₂ / bis-(2-methoxy-ethyl) ether / Heating

2.2: 41 percent / DMAP / 24 h / 20 °C

3.1: 100 percent / N-bromosuccinimide / CCl₄ / 1.5 h / Heating

4.1: KO-t-Bu

5.1: cerium ammonium nitrate

6.1: CF₃COOH / CH₂Cl₂ / 2 h / 20 °C

With N-Bromosuccinimide; ammonium cerium(IV) nitrate; potassium tert-butylate; hydrogen; SULFAMIDE; trifluoroacetic acid; Ra-Ni; In tetrahydrofuran; tetrachloromethane; dichloromethane; diethylene glycol dimethyl ether; 1.1: Catalytic hydrogenation / 2.1: Cyclization / 2.2: Acylation / 3.1: Bromination / 4.1: Substitution / 4.2: Cyclization / 5.1: Oxidation / 6.1: Hydrolysis;
DOI:10.1021/ja0005136

Reference yield:

: 186039-77-0
1,4-dimethoxy-5,6-dimethyl-2,3-diaminobenzene

: 271800-39-6
C₄₀H₅₂N₆O₆S

Guidance literature:: Multi-step reaction with 5 steps

1.1: SO₂NH₂ / bis-(2-methoxy-ethyl) ether / Heating

1.2: 41 percent / DMAP / 24 h / 20 °C

2.1: 100 percent / N-bromosuccinimide / CCl₄ / 1.5 h / Heating

3.1: KO-t-Bu

4.1: cerium ammonium nitrate

5.1: CF₃COOH / CH₂Cl₂ / 2 h / 20 °C

With N-Bromosuccinimide; ammonium cerium(IV) nitrate; potassium tert-butylate; SULFAMIDE; trifluoroacetic acid; In tetrachloromethane; dichloromethane; diethylene glycol dimethyl ether; 1.1: Cyclization / 1.2: Acylation / 2.1: Bromination / 3.1: Substitution / 3.2: Cyclization / 4.1: Oxidation / 5.1: Hydrolysis;
DOI:10.1021/ja0005136