(E)-1-[4-(5-phenyl-1-trimethylsilyl-2-penten-1-yl)phenyl]ethanone

Base Information

• Chemical Name: (E)-1-[4-(5-phenyl-1-trimethylsilyl-2-penten-1-yl)phenyl]ethanone
• CAS No.: 1237538-54-3
• Molecular Formula: C₂₂H₂₈OSi
• Molecular Weight: 336.549
• Mol file: 1237538-54-3.mol

Synonyms:(E)-1-[4-(5-phenyl-1-trimethylsilyl-2-penten-1-yl)phenyl]ethanone

Chemical Property of (E)-1-[4-(5-phenyl-1-trimethylsilyl-2-penten-1-yl)phenyl]ethanone

Chemical Property:

Purity/Quality:

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Technology Process of (E)-1-[4-(5-phenyl-1-trimethylsilyl-2-penten-1-yl)phenyl]ethanone

There total 2 articles about (E)-1-[4-(5-phenyl-1-trimethylsilyl-2-penten-1-yl)phenyl]ethanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

(E)-5-phenyl-1-trimethylsilyl-1-penten-3-yl 2-methoxybenzoate (1237539-30-8) + 4-acetylphenylboronic acid (149104-90-5) → (E)-1-[4-(5-phenyl-1-trimethylsilyl-2-penten-1-yl)phenyl]ethanone (1237538-54-3) + C27H26O4

Guidance literature:

With silver hexafluoroantimonate; 1,10-Phenanthroline; palladium diacetate; p-benzoquinone; In 1,2-dichloro-ethane; at 25 - 60 ℃; regioselective reaction;

DOI:10.1021/ol101114r

Reference yield: 64.0%

(E)-5-phenyl-1-trimethylsilyl-1-penten-3-yl 2-methoxybenzoate (1237539-30-8) + 4-acetylphenylboronic acid (149104-90-5) → (E)-1-[4-(5-phenyl-1-trimethylsilyl-2-penten-1-yl)phenyl]ethanone (1237538-54-3)

Guidance literature:

With silver hexafluoroantimonate; bathophenanthroline; palladium diacetate; In tetrahydrofuran; at 25 - 60 ℃; regioselective reaction;

DOI:10.1021/ol101114r

upstream raw materials:

(E)-5-phenyl-1-trimethylsilyl-1-penten-3-yl 2-methoxybenzoate

4-acetylphenylboronic acid