(2R,3R)-2-((R)-2-Acetylamino-3-phenyl-propionylamino)-3-hydroxy-butyric acid

Base Information

Chemical Name:(2R,3R)-2-((R)-2-Acetylamino-3-phenyl-propionylamino)-3-hydroxy-butyric acid
CAS No.:138588-07-5
Molecular Formula:C₁₅H₂₀N₂O₅
Molecular Weight:308.334
Hs Code.:

Synonyms:(2R,3R)-2-((R)-2-Acetylamino-3-phenyl-propionylamino)-3-hydroxy-butyric acid

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Chemical Property of (2R,3R)-2-((R)-2-Acetylamino-3-phenyl-propionylamino)-3-hydroxy-butyric acid

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Technology Process of (2R,3R)-2-((R)-2-Acetylamino-3-phenyl-propionylamino)-3-hydroxy-butyric acid

There total 2 articles about (2R,3R)-2-((R)-2-Acetylamino-3-phenyl-propionylamino)-3-hydroxy-butyric acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 138588-06-4
(2R,3R)-2-((R)-2-Acetylamino-3-phenyl-propionylamino)-3-hydroxy-butyric acid benzyl ester

: 138588-07-5
(2R,3R)-2-((R)-2-Acetylamino-3-phenyl-propionylamino)-3-hydroxy-butyric acid

Guidance literature:: With hydrogen; palladium on activated charcoal; In methanol; for 6h; under 760 Torr; Ambient temperature;
DOI:10.1016/0040-4039(91)80238-2

Reference yield:

: 10172-89-1
(R)-N-acetylphenylalanin

: 138588-07-5
(2R,3R)-2-((R)-2-Acetylamino-3-phenyl-propionylamino)-3-hydroxy-butyric acid

Guidance literature:: Multi-step reaction with 2 steps

1: 70 percent / DCC, HOBt / CH₂Cl₂ / 18 h / Ambient temperature

2: H₂ / 10percent Pd/C / methanol / 6 h / 760 Torr / Ambient temperature

With hydrogen; benzotriazol-1-ol; dicyclohexyl-carbodiimide; palladium on activated charcoal; In methanol; dichloromethane;
DOI:10.1016/0040-4039(91)80238-2

Reference yield: 43.0%

: 138588-07-5
(2R,3R)-2-((R)-2-Acetylamino-3-phenyl-propionylamino)-3-hydroxy-butyric acid

: 138588-04-2
Acetic acid (2R,3R,4R,5S,6S)-2-[(S)-2-((R)-2-amino-propionylamino)-propoxy]-4,5-dimethoxy-6-methyl-tetrahydro-pyran-3-yl ester

: 138588-08-6
Acetic acid (2R,3R,4R,5S,6S)-2-((S)-2-{(R)-2-[(2R,3R)-2-((R)-2-acetylamino-3-phenyl-propionylamino)-3-hydroxy-butyrylamino]-propionylamino}-propoxy)-4,5-dimethoxy-6-methyl-tetrahydro-pyran-3-yl ester

Guidance literature:: With benzotriazol-1-ol; dicyclohexyl-carbodiimide; In acetonitrile; for 18h; Ambient temperature;
DOI:10.1016/0040-4039(91)80238-2