(2R,3R)-2-((R)-2-Acetylamino-3-phenyl-propionylamino)-3-hydroxy-butyric acid benzyl ester

Base Information

Chemical Name:(2R,3R)-2-((R)-2-Acetylamino-3-phenyl-propionylamino)-3-hydroxy-butyric acid benzyl ester
CAS No.:138588-06-4
Molecular Formula:C₂₂H₂₆N₂O₅
Molecular Weight:398.459
Hs Code.:

Synonyms:(2R,3R)-2-((R)-2-Acetylamino-3-phenyl-propionylamino)-3-hydroxy-butyric acid benzyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2R,3R)-2-((R)-2-Acetylamino-3-phenyl-propionylamino)-3-hydroxy-butyric acid benzyl ester

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Technology Process of (2R,3R)-2-((R)-2-Acetylamino-3-phenyl-propionylamino)-3-hydroxy-butyric acid benzyl ester

There total 1 articles about (2R,3R)-2-((R)-2-Acetylamino-3-phenyl-propionylamino)-3-hydroxy-butyric acid benzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 10172-89-1
(R)-N-acetylphenylalanin

: 138588-05-3
D-threonine benzyl ester

: 138588-06-4
(2R,3R)-2-((R)-2-Acetylamino-3-phenyl-propionylamino)-3-hydroxy-butyric acid benzyl ester

Guidance literature:: With benzotriazol-1-ol; dicyclohexyl-carbodiimide; In dichloromethane; for 18h; Ambient temperature;
DOI:10.1016/0040-4039(91)80238-2

Reference yield:

: 138588-06-4
(2R,3R)-2-((R)-2-Acetylamino-3-phenyl-propionylamino)-3-hydroxy-butyric acid benzyl ester

: 138588-07-5
(2R,3R)-2-((R)-2-Acetylamino-3-phenyl-propionylamino)-3-hydroxy-butyric acid

Guidance literature:: With hydrogen; palladium on activated charcoal; In methanol; for 6h; under 760 Torr; Ambient temperature;
DOI:10.1016/0040-4039(91)80238-2

Reference yield:

: 138588-06-4
(2R,3R)-2-((R)-2-Acetylamino-3-phenyl-propionylamino)-3-hydroxy-butyric acid benzyl ester

: 138588-08-6
Acetic acid (2R,3R,4R,5S,6S)-2-((S)-2-{(R)-2-[(2R,3R)-2-((R)-2-acetylamino-3-phenyl-propionylamino)-3-hydroxy-butyrylamino]-propionylamino}-propoxy)-4,5-dimethoxy-6-methyl-tetrahydro-pyran-3-yl ester

Guidance literature:: Multi-step reaction with 2 steps

1: H₂ / 10percent Pd/C / methanol / 6 h / 760 Torr / Ambient temperature

2: 43 percent / DCC, HOBt / acetonitrile / 18 h / Ambient temperature

With hydrogen; benzotriazol-1-ol; dicyclohexyl-carbodiimide; palladium on activated charcoal; In methanol; acetonitrile;
DOI:10.1016/0040-4039(91)80238-2