(3S,4R,6S,7S)-7-(tert-butyldimethylsilyloxy)-4-(4-methoxybenzyloxy)-3,6-dimethyloctanal

Base Information

Chemical Name:(3S,4R,6S,7S)-7-(tert-butyldimethylsilyloxy)-4-(4-methoxybenzyloxy)-3,6-dimethyloctanal
CAS No.:1234707-93-7
Molecular Formula:C₂₄H₄₂O₄Si
Molecular Weight:422.681
Hs Code.:

Synonyms:(3S,4R,6S,7S)-7-(tert-butyldimethylsilyloxy)-4-(4-methoxybenzyloxy)-3,6-dimethyloctanal

Suppliers and Price of (3S,4R,6S,7S)-7-(tert-butyldimethylsilyloxy)-4-(4-methoxybenzyloxy)-3,6-dimethyloctanal

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of (3S,4R,6S,7S)-7-(tert-butyldimethylsilyloxy)-4-(4-methoxybenzyloxy)-3,6-dimethyloctanal

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (3S,4R,6S,7S)-7-(tert-butyldimethylsilyloxy)-4-(4-methoxybenzyloxy)-3,6-dimethyloctanal

There total 1 articles about (3S,4R,6S,7S)-7-(tert-butyldimethylsilyloxy)-4-(4-methoxybenzyloxy)-3,6-dimethyloctanal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 1234707-92-6
(3S,4R,6S,7S)-7-(tert-butyldimethylsilyloxy)-4-(4-methoxybenzyloxy)-3,6-dimethyloctan-1-ol

: 1234707-93-7
(3S,4R,6S,7S)-7-(tert-butyldimethylsilyloxy)-4-(4-methoxybenzyloxy)-3,6-dimethyloctanal

Guidance literature:: (3S,4R,6S,7S)-7-(tert-butyldimethylsilyloxy)-4-(4-methoxybenzyloxy)-3,6-dimethyloctan-1-ol; With oxalyl dichloride; dimethyl sulfoxide; In dichloromethane; at -78 ℃; for 0.5h; Inert atmosphere;

With triethylamine; In dichloromethane; at -78 - 20 ℃; Inert atmosphere;
DOI:10.1021/ol1011423

Reference yield: 95.0%

: 1234707-93-7
(3S,4R,6S,7S)-7-(tert-butyldimethylsilyloxy)-4-(4-methoxybenzyloxy)-3,6-dimethyloctanal

: 2065-66-9
methyl-triphenylphosphonium iodide

: 1234707-85-7
tert-butyl((2S,3S,5R,6S)-5-(4-methoxybenzyloxy)-3,6-dimethylnon-8-en-2-yloxy)dimethylsilane

Guidance literature:: methyl-triphenylphosphonium iodide; With n-butyllithium; In tetrahydrofuran; Inert atmosphere;

(3S,4R,6S,7S)-7-(tert-butyldimethylsilyloxy)-4-(4-methoxybenzyloxy)-3,6-dimethyloctanal; In tetrahydrofuran; at 20 ℃; Inert atmosphere;
DOI:10.1021/ol1011423