5-amino-N-(1-ethyl-1H-hexahydroazepin-3-yl)-2-methoxy-4-methylaminobenzamide

Base Information

Chemical Name:5-amino-N-(1-ethyl-1H-hexahydroazepin-3-yl)-2-methoxy-4-methylaminobenzamide
CAS No.:179535-18-3
Molecular Formula:C₁₇H₂₈N₄O₂
Molecular Weight:320.435
Hs Code.:

Synonyms:5-amino-N-(1-ethyl-1H-hexahydroazepin-3-yl)-2-methoxy-4-methylaminobenzamide

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Chemical Property of 5-amino-N-(1-ethyl-1H-hexahydroazepin-3-yl)-2-methoxy-4-methylaminobenzamide

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Technology Process of 5-amino-N-(1-ethyl-1H-hexahydroazepin-3-yl)-2-methoxy-4-methylaminobenzamide

There total 6 articles about 5-amino-N-(1-ethyl-1H-hexahydroazepin-3-yl)-2-methoxy-4-methylaminobenzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 179534-98-6
1-ethyl-N-(1-ethyl-1H-hexahydroazepin-3-yl)-6-methoxy-1H-benzotriazole-5-carboxamide

: 179535-18-3
5-amino-N-(1-ethyl-1H-hexahydroazepin-3-yl)-2-methoxy-4-methylaminobenzamide

Guidance literature:: With acetic acid; sodium nitrite;

Reference yield:

: 179535-17-2
N-(1-ethyl-1H-hexahydroazepin-3-yl)-2-methoxy-4-methylamino-5-nitrobenzamide

: 179535-18-3
5-amino-N-(1-ethyl-1H-hexahydroazepin-3-yl)-2-methoxy-4-methylaminobenzamide

Guidance literature:: With hydrogen; palladium on activated charcoal;
DOI:10.1016/S0960-894X(98)00341-2

Reference yield:

: 68255-77-6
2-methoxy-4-chloro-5-nitrobenzoic acid

: 179535-18-3
5-amino-N-(1-ethyl-1H-hexahydroazepin-3-yl)-2-methoxy-4-methylaminobenzamide

Guidance literature:: Multi-step reaction with 4 steps

1: SOCl₂

4: H₂ / Pd/C

With thionyl chloride; hydrogen; palladium on activated charcoal;
DOI:10.1016/S0960-894X(98)00341-2