C₃₀H₃₃N₃O₃

Base Information

Chemical Name:C₃₀H₃₃N₃O₃
CAS No.:900518-68-5
Molecular Formula:C₃₀H₃₃N₃O₃
Molecular Weight:483.61
Hs Code.:

C<sub>30</sub>H<sub>33</sub>N<sub>3</sub>O<sub>3</sub>

Synonyms:C₃₀H₃₃N₃O₃

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Chemical Property of C₃₀H₃₃N₃O₃

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Technology Process of C₃₀H₃₃N₃O₃

There total 10 articles about C₃₀H₃₃N₃O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 900518-67-4
C₂₉H₃₃BrN₂O₃

: copper(l) cyanide

: 900518-68-5
C₃₀H₃₃N₃O₃

Guidance literature:: In N,N-dimethyl-formamide; at 120 ℃; for 20h; Inert atmosphere;
DOI:10.1016/j.tetlet.2013.01.003

Reference yield:

: 26420-79-1
1-chloro-3-benzyloxypropane

: 900518-68-5
C₃₀H₃₃N₃O₃

Guidance literature:: Multi-step reaction with 9 steps

1: N-ethyl-N,N-diisopropylamine; sodium iodide / N,N-dimethyl-formamide / 3.5 h / 100 °C

2: trichlorophosphate / 4 h / 25 - 35 °C

3: bromine / dichloromethane / 2.5 h / 0 °C

4: dichloromethane; toluene / 16 h / Reflux

5: sodium hydroxide / methanol; water / 3 h / 40 °C

6: triethylamine; hydrogen / methanol / 2 h / 70 °C / 6080.41 - 7600.51 Torr / Autoclave; Inert atmosphere

7: N-ethyl-N,N-diisopropylamine; diphenyl phosphoryl azide / toluene / 1 h / 70 °C

8: 10 h / 95 °C

9: N,N-dimethyl-formamide / 20 h / 120 °C / Inert atmosphere

With diphenyl phosphoryl azide; hydrogen; bromine; triethylamine; N-ethyl-N,N-diisopropylamine; sodium iodide; sodium hydroxide; trichlorophosphate; In methanol; dichloromethane; water; N,N-dimethyl-formamide; toluene; 2: |Vilsmeier-Haack Formylation / 4: |Wittig Olefination;
DOI:10.1016/j.tetlet.2013.01.003

Reference yield:

: 496-15-1
1-indoline

: 900518-68-5
C₃₀H₃₃N₃O₃

Guidance literature:: Multi-step reaction with 9 steps

1: N-ethyl-N,N-diisopropylamine; sodium iodide / N,N-dimethyl-formamide / 3.5 h / 100 °C

2: trichlorophosphate / 4 h / 25 - 35 °C

3: bromine / dichloromethane / 2.5 h / 0 °C

4: dichloromethane; toluene / 16 h / Reflux

5: sodium hydroxide / methanol; water / 3 h / 40 °C

6: triethylamine; hydrogen / methanol / 2 h / 70 °C / 6080.41 - 7600.51 Torr / Autoclave; Inert atmosphere

7: N-ethyl-N,N-diisopropylamine; diphenyl phosphoryl azide / toluene / 1 h / 70 °C

8: 10 h / 95 °C

9: N,N-dimethyl-formamide / 20 h / 120 °C / Inert atmosphere

With diphenyl phosphoryl azide; hydrogen; bromine; triethylamine; N-ethyl-N,N-diisopropylamine; sodium iodide; sodium hydroxide; trichlorophosphate; In methanol; dichloromethane; water; N,N-dimethyl-formamide; toluene; 2: |Vilsmeier-Haack Formylation / 4: |Wittig Olefination;
DOI:10.1016/j.tetlet.2013.01.003