cis-4-(tert-butyldiphenylsiloxy)-1-{5-[4-(tert-butyldiphenylsiloxy)-1-hydroxybutyl]tetrahydrofuran-2-yl}butan-1-ol

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Chemical Name:cis-4-(tert-butyldiphenylsiloxy)-1-{5-[4-(tert-butyldiphenylsiloxy)-1-hydroxybutyl]tetrahydrofuran-2-yl}butan-1-ol
CAS No.:909767-35-7
Molecular Formula:C₄₄H₆₀O₅Si₂
Molecular Weight:725.128
Hs Code.:

Synonyms:cis-4-(tert-butyldiphenylsiloxy)-1-{5-[4-(tert-butyldiphenylsiloxy)-1-hydroxybutyl]tetrahydrofuran-2-yl}butan-1-ol

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Chemical Property of cis-4-(tert-butyldiphenylsiloxy)-1-{5-[4-(tert-butyldiphenylsiloxy)-1-hydroxybutyl]tetrahydrofuran-2-yl}butan-1-ol

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Technology Process of cis-4-(tert-butyldiphenylsiloxy)-1-{5-[4-(tert-butyldiphenylsiloxy)-1-hydroxybutyl]tetrahydrofuran-2-yl}butan-1-ol

There total 6 articles about cis-4-(tert-butyldiphenylsiloxy)-1-{5-[4-(tert-butyldiphenylsiloxy)-1-hydroxybutyl]tetrahydrofuran-2-yl}butan-1-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 909767-34-6
C₄₄H₅₈O₂Si₂

: 909767-35-7
cis-4-(tert-butyldiphenylsiloxy)-1-{5-[4-(tert-butyldiphenylsiloxy)-1-hydroxybutyl]tetrahydrofuran-2-yl}butan-1-ol

Guidance literature:: With sodium periodate; ruthenium trichloride; In tetrahydrofuran; water; at 0 ℃; for 6h;
DOI:10.1021/ol060520k

Reference yield:

: 131392-77-3
(4E,8E)-dodeca-4,8-diene-1,12-diol

: 909767-35-7
cis-4-(tert-butyldiphenylsiloxy)-1-{5-[4-(tert-butyldiphenylsiloxy)-1-hydroxybutyl]tetrahydrofuran-2-yl}butan-1-ol

Guidance literature:: Multi-step reaction with 2 steps

1: 24.4 g / i-Pr₂EtN / CH₂Cl₂ / 24 h / 20 °C

2: 83 percent / sodium periodate / ruthenium trichloride / tetrahydrofuran; H₂O / 6 h / 0 °C

With sodium periodate; N-ethyl-N,N-diisopropylamine; ruthenium trichloride; In tetrahydrofuran; dichloromethane; water;
DOI:10.1021/ol060520k

Reference yield:

: 837382-45-3
trans,trans-5,9-Cyclododecadien-1,2-diol

: 909767-35-7
cis-4-(tert-butyldiphenylsiloxy)-1-{5-[4-(tert-butyldiphenylsiloxy)-1-hydroxybutyl]tetrahydrofuran-2-yl}butan-1-ol

Guidance literature:: Multi-step reaction with 4 steps

1: NaIO₄; water / CH₂Cl₂; acetone

2: NaBH₄ / methanol / 0 °C

3: 24.4 g / i-Pr₂EtN / CH₂Cl₂ / 24 h / 20 °C

4: 83 percent / sodium periodate / ruthenium trichloride / tetrahydrofuran; H₂O / 6 h / 0 °C

With sodium tetrahydroborate; sodium periodate; water; N-ethyl-N,N-diisopropylamine; ruthenium trichloride; In tetrahydrofuran; methanol; dichloromethane; water; acetone;
DOI:10.1021/ol060520k