6-N-benzoyl-9-[3,5-bis(tert-butyldimethylsilanyloxymethyl)phenyl]adenine

Base Information

Chemical Name:6-N-benzoyl-9-[3,5-bis(tert-butyldimethylsilanyloxymethyl)phenyl]adenine
CAS No.:867259-37-8
Molecular Formula:C₃₂H₄₅N₅O₃Si₂
Molecular Weight:603.912
Hs Code.:

Synonyms:6-N-benzoyl-9-[3,5-bis(tert-butyldimethylsilanyloxymethyl)phenyl]adenine

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Chemical Property of 6-N-benzoyl-9-[3,5-bis(tert-butyldimethylsilanyloxymethyl)phenyl]adenine

Chemical Property:

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Technology Process of 6-N-benzoyl-9-[3,5-bis(tert-butyldimethylsilanyloxymethyl)phenyl]adenine

There total 5 articles about 6-N-benzoyl-9-[3,5-bis(tert-butyldimethylsilanyloxymethyl)phenyl]adenine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 49.0%

: 867259-36-7
9-[3,5-bis(tert-butyldimethylsilanyloxymethyl)phenyl]adenine

: 98-88-4
benzoyl chloride

: 867259-37-8
6-N-benzoyl-9-[3,5-bis(tert-butyldimethylsilanyloxymethyl)phenyl]adenine

Guidance literature:: With pyridine; at 20 ℃; for 3h;
DOI:10.1021/jo050635m

Reference yield:

: 867259-33-4
5-amino-4-[3,5-bis(hydroxymethyl)anilino]-6-chloropyrimidine

: 867259-37-8
6-N-benzoyl-9-[3,5-bis(tert-butyldimethylsilanyloxymethyl)phenyl]adenine

Guidance literature:: Multi-step reaction with 4 steps

1: 70 percent / imidazole / dimethylformamide / 24 h / 20 °C

2: 77 percent / acetic anhydride / 6 h / Heating

3: 63 percent / NH₃ gas; MeOH / 6 h / 90 °C

4: 49 percent / pyridine / 3 h / 20 °C

With pyridine; 1H-imidazole; methanol; ammonia; acetic anhydride; In N,N-dimethyl-formamide;
DOI:10.1021/jo050635m

Reference yield:

: 71176-54-0
(3-amino-5-hydroxymethylphenyl)methanol

: 867259-37-8
6-N-benzoyl-9-[3,5-bis(tert-butyldimethylsilanyloxymethyl)phenyl]adenine

Guidance literature:: Multi-step reaction with 5 steps

1: 86 percent / aq. HCl / ethanol / 7 h / Heating

2: 70 percent / imidazole / dimethylformamide / 24 h / 20 °C

3: 77 percent / acetic anhydride / 6 h / Heating

4: 63 percent / NH₃ gas; MeOH / 6 h / 90 °C

5: 49 percent / pyridine / 3 h / 20 °C

With pyridine; 1H-imidazole; hydrogenchloride; methanol; ammonia; acetic anhydride; In ethanol; N,N-dimethyl-formamide;
DOI:10.1021/jo050635m