Ophiopogonanone A

Base Information

Chemical Name:Ophiopogonanone A
CAS No.:75239-63-3
Molecular Formula:C₁₈H₁₆O₆
Molecular Weight:328.321
Hs Code.:
DSSTox Substance ID:DTXSID40433934
Nikkaji Number:J976.609J
Wikidata:Q27155073
Mol file:75239-63-3.mol

Synonyms:Ophiopogonanone A;Ophiogonanone A;75239-63-3;3-(1,3-benzodioxol-5-ylmethyl)-5,7-dihydroxy-6-methyl-2,3-dihydrochromen-4-one;CHEBI:81117;DTXSID40433934;AKOS032949040;C17475;Q-100811;Q27155073;3-[(2H-1,3-Benzodioxol-5-yl)methyl]-5,7-dihydroxy-6-methyl-2,3-dihydro-4H-1-benzopyran-4-one

Suppliers and Price of Ophiopogonanone A

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Usbiological
Ophiopogonanone A
10mg
$ 581.00

Crysdot
OphiopogonanoneA 95+%
5mg
$ 860.00

AvaChem
Ophiogonanone A
10mg
$ 790.00

AvaChem
Ophiogonanone A
5mg
$ 390.00

Arctom
OphiopogonanoneA
5mg
$ 339.00

Total 20 raw suppliers

Chemical Property of Ophiopogonanone A

Chemical Property:

Vapor Pressure:0mmHg at 25°C
Boiling Point:581.829°C at 760 mmHg
PKA:7.89±0.40(Predicted)
Flash Point:216.967°C
PSA：85.22000
Density:1.450
LogP:2.56890
XLogP3:3.4
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:6
Rotatable Bond Count:2
Exact Mass:328.09468823
Heavy Atom Count:24
Complexity:482

Purity/Quality:

99%, ^*data from raw suppliers

Ophiopogonanone A ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=C(C2=C(C=C1O)OCC(C2=O)CC3=CC4=C(C=C3)OCO4)O

Technology Process of Ophiopogonanone A

There total 7 articles about Ophiopogonanone A which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

: 106929-62-8
3-<(1,3-benzodioxol-5-yl)methyl>-7-benzyloxy-5-hydroxy-6-methyl-4H-1-benzopyran-4-on

: 106929-70-8,75239-63-3
ophiopogonanone A

Guidance literature:: With hydrogen; palladium on activated charcoal; In acetone; for 24h;

Reference yield:

: 120-57-0,30024-74-9
piperonal

: 106929-70-8,75239-63-3
ophiopogonanone A

Guidance literature:: Multi-step reaction with 6 steps

1: 1) piperidine; 2) 0.25 N NaOEt / 1) 72 h, heating; 2) heating

2: 70 percent / H₂ / 10percent Pd/C / acetone

3: 66 percent / K₂CO₃/NaI / acetone / 8 h / Heating

4: 66 percent / K₂CO₃/NaI / acetone / 8 h / Heating

5: 1) Na; 2) 10 percent HCl / 1.) 0 deg C, 16 h, 2.) MeOH, reflux

6: 55 percent / H₂ / 10percent Pd/C / acetone / 24 h

With piperidine; hydrogenchloride; hydrogen; sodium ethanolate; sodium; potassium carbonate; sodium iodide; palladium on activated charcoal; In acetone;

Reference yield:

: 2657-28-5
2,4,6-trihydroxy-3-methyl-acetophenon

: 106929-70-8,75239-63-3
ophiopogonanone A

Guidance literature:: Multi-step reaction with 7 steps

1: 34 percent / K₂CO₃ / acetone / 1 h / 0 °C

2: 1) piperidine; 2) 0.25 N NaOEt / 1) 72 h, heating; 2) heating

3: 70 percent / H₂ / 10percent Pd/C / acetone

4: 66 percent / K₂CO₃/NaI / acetone / 8 h / Heating

5: 66 percent / K₂CO₃/NaI / acetone / 8 h / Heating

6: 1) Na; 2) 10 percent HCl / 1.) 0 deg C, 16 h, 2.) MeOH, reflux

7: 55 percent / H₂ / 10percent Pd/C / acetone / 24 h

With piperidine; hydrogenchloride; hydrogen; sodium ethanolate; sodium; potassium carbonate; sodium iodide; palladium on activated charcoal; In acetone;