N-ε-benzyloxycarbonyl-N-α-tert-butoxycarbonyl-L-lysinyl-D-alanyl-D-alanine benzyl ester

Base Information

Chemical Name:N-ε-benzyloxycarbonyl-N-α-tert-butoxycarbonyl-L-lysinyl-D-alanyl-D-alanine benzyl ester
CAS No.:18814-54-5
Molecular Formula:C₃₂H₄₄N₄O₈
Molecular Weight:612.723
Hs Code.:

Synonyms:N-ε-benzyloxycarbonyl-N-α-tert-butoxycarbonyl-L-lysinyl-D-alanyl-D-alanine benzyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-ε-benzyloxycarbonyl-N-α-tert-butoxycarbonyl-L-lysinyl-D-alanyl-D-alanine benzyl ester

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Technology Process of N-ε-benzyloxycarbonyl-N-α-tert-butoxycarbonyl-L-lysinyl-D-alanyl-D-alanine benzyl ester

There total 2 articles about N-ε-benzyloxycarbonyl-N-α-tert-butoxycarbonyl-L-lysinyl-D-alanyl-D-alanine benzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 32.0%

: 2389-45-9
Boc-Lys(Z)-OH

: D-alanyl-D-alanine benzyl ester trifluoroacetic acid salt

: 18814-54-5
N-ε-benzyloxycarbonyl-N-α-tert-butoxycarbonyl-L-lysinyl-D-alanyl-D-alanine benzyl ester

Guidance literature:: With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In dichloromethane; at 0 - 20 ℃; for 15h;
DOI:10.1021/jo035583k

Reference yield:

: 18814-54-5
α-BOC-ε-Z-Lys-D-Ala-D-Ala-OBzl

Guidance literature:: Peptid (I) 1. + 2. α-tert-Butoxy-carbonyl-ε-benzyloxy-carbonyllysin, Dicyclohexylcarbodiimid;
DOI:10.1021/bi00742a004

Reference yield: 100.0%

: 18814-54-5
N-ε-benzyloxycarbonyl-N-α-tert-butoxycarbonyl-L-lysinyl-D-alanyl-D-alanine benzyl ester

: ClH*C₂₇H₃₆N₄O₆

Guidance literature:: N-ε-benzyloxycarbonyl-N-α-tert-butoxycarbonyl-L-lysinyl-D-alanyl-D-alanine benzyl ester; With trifluoroacetic acid; at 20 ℃; Inert atmosphere;

With hydrogenchloride; In diethyl ether; at 20 ℃; Inert atmosphere;
DOI:10.1002/asia.201601357