2,2,6,6-Tetramethyl-4,8-bis(4-methylphenyl)-3,7-bis(trimethylsilyl)-1,5-dioxa-2,6-disila-3,7-cyclooctadiene

Base Information

Chemical Name:2,2,6,6-Tetramethyl-4,8-bis(4-methylphenyl)-3,7-bis(trimethylsilyl)-1,5-dioxa-2,6-disila-3,7-cyclooctadiene
CAS No.:123725-21-3
Molecular Formula:C₂₈H₄₄O₂Si₄
Molecular Weight:524.998
Hs Code.:

Synonyms:2,2,6,6-Tetramethyl-4,8-bis(4-methylphenyl)-3,7-bis(trimethylsilyl)-1,5-dioxa-2,6-disila-3,7-cyclooctadiene

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Chemical Property of 2,2,6,6-Tetramethyl-4,8-bis(4-methylphenyl)-3,7-bis(trimethylsilyl)-1,5-dioxa-2,6-disila-3,7-cyclooctadiene

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Technology Process of 2,2,6,6-Tetramethyl-4,8-bis(4-methylphenyl)-3,7-bis(trimethylsilyl)-1,5-dioxa-2,6-disila-3,7-cyclooctadiene

There total 2 articles about 2,2,6,6-Tetramethyl-4,8-bis(4-methylphenyl)-3,7-bis(trimethylsilyl)-1,5-dioxa-2,6-disila-3,7-cyclooctadiene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 32.0%

: 123725-18-8
2-Diazo-1-(4-methylphenyl)-2-(pentamethyldisilanyl)-ethanone

: 123725-21-3
2,2,6,6-Tetramethyl-4,8-bis(4-methylphenyl)-3,7-bis(trimethylsilyl)-1,5-dioxa-2,6-disila-3,7-cyclooctadiene

Guidance literature:: In benzene; Irradiation;

Reference yield:

: 17263-64-8
2-diazo-1-(4-methylphenyl)ethanone

: 123725-21-3
2,2,6,6-Tetramethyl-4,8-bis(4-methylphenyl)-3,7-bis(trimethylsilyl)-1,5-dioxa-2,6-disila-3,7-cyclooctadiene

Guidance literature:: Multi-step reaction with 2 steps

1: 76 percent / EtNiPr₂ / diethyl ether / 1) 30 min, 0 deg C 2) 2-5h, room temperature

2: 32 percent / benzene / Irradiation

With N-ethyl-N,N-diisopropylamine; In diethyl ether; benzene;