1,4,5-trimethylimidazole-tris(pentafluorophenyl)borane adduct

Base Information

• Chemical Name: 1,4,5-trimethylimidazole-tris(pentafluorophenyl)borane adduct
• CAS No.: 618442-71-0
• Molecular Formula: C₂₄H₁₀BF₁₅N₂
• Molecular Weight: 622.144
• Mol file: 618442-71-0.mol

Synonyms:1,4,5-trimethylimidazole-tris(pentafluorophenyl)borane adduct

Chemical Property of 1,4,5-trimethylimidazole-tris(pentafluorophenyl)borane adduct

Chemical Property:

Purity/Quality:

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Technology Process of 1,4,5-trimethylimidazole-tris(pentafluorophenyl)borane adduct

There total 1 articles about 1,4,5-trimethylimidazole-tris(pentafluorophenyl)borane adduct which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

1,4,5-Trimethylimidazole (20185-22-2) + tris(pentafluorophenyl)borate (1109-15-5) → 1,4,5-trimethylimidazole-tris(pentafluorophenyl)borane adduct (618442-71-0)

Guidance literature:

In pentane; under Ar; suspn. of imidazole in pentane cooled to 0°C, reacted with equiv. amt. of B(C6F5)3, stirred for 12 h at room temp.; solid filtered off and dried under vac.; elem. anal.;

DOI:10.1039/b210030b

Reference yield: 89.0%

1,4,5-trimethylimidazole-tris(pentafluorophenyl)borane adduct (618442-71-0) → B(C6F5)2C6F4CH3N2C3(CH3)2

Guidance literature:

With methyllithium; In tetrahydrofuran; benzene; byproducts: CH4, LiF; under Ar; mixt. of benzene/THF (10/1) added to mixt. of B compd. and MeLi, stirred for 12; solvents removed under vac., benzene added, LiF filtered off, filtrate evapd.; elem. anal.;

DOI:10.1039/b210030b

upstream raw materials:

1,4,5-Trimethylimidazole

tris(pentafluorophenyl)borate