Ru^IICl₃(DMSO)(4-(3'-chloro-4'-fluoroanilino)-6-(2-(2-aminoethyl)aminoethoxy)-7-methoxyquinazoline)

Base Information

• Chemical Name: Ru^IICl₃(DMSO)(4-(3'-chloro-4'-fluoroanilino)-6-(2-(2-aminoethyl)aminoethoxy)-7-methoxyquinazoline)
• CAS No.: 1373945-06-2
• Molecular Formula: C₂₁H₂₇Cl₄FN₅O₃RuS
• Molecular Weight: 691.423

Synonyms:Ru^IICl₃(DMSO)(4-(3'-chloro-4'-fluoroanilino)-6-(2-(2-aminoethyl)aminoethoxy)-7-methoxyquinazoline)

Chemical Property of Ru^IICl₃(DMSO)(4-(3'-chloro-4'-fluoroanilino)-6-(2-(2-aminoethyl)aminoethoxy)-7-methoxyquinazoline)

Chemical Property:

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Technology Process of Ru^IICl₃(DMSO)(4-(3'-chloro-4'-fluoroanilino)-6-(2-(2-aminoethyl)aminoethoxy)-7-methoxyquinazoline)

There total 1 articles about Ru^IICl₃(DMSO)(4-(3'-chloro-4'-fluoroanilino)-6-(2-(2-aminoethyl)aminoethoxy)-7-methoxyquinazoline) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

Hydrogen trans-Bis(dimethhyl sulfoxide) tetrachlororuthenate(III) + 6-(2-(2-aminoethylamino)ethoxy)-4-(3-chloro-4-fluoro-phenylamino)-7-methoxy quinazoline (1360859-35-3) → RuIICl3(DMSO)(4-(3'-chloro-4'-fluoroanilino)-6-(2-(2-aminoethyl)aminoethoxy)-7-methoxyquinazoline) (1373945-06-2)

Guidance literature:

Hydrogen trans-Bis(dimethhyl sulfoxide) tetrachlororuthenate(III); 6-(2-(2-aminoethylamino)ethoxy)-4-(3-chloro-4-fluoro-phenylamino)-7-methoxy quinazoline; In ethanol; acetonitrile; at 20 ℃; for 0.5h;

With water; In ethanol; acetonitrile; for 0.5h;

DOI:10.1016/j.ejmech.2014.02.062

Reference yield:

RuIICl3(DMSO)(4-(3'-chloro-4'-fluoroanilino)-6-(2-(2-aminoethyl)aminoethoxy)-7-methoxyquinazoline) (1373945-06-2) → 6-(2-(2-aminoethylamino)ethoxy)-4-(3-chloro-4-fluoro-phenylamino)-7-methoxy quinazoline (1360859-35-3) + RuIIICl2(DMSO)(4-(3'-chloro-4'-fluoroanilino)-6-(2-(2-aminoethyl)aminoethoxy)-7-methoxyquinazoline)(H2O)

Guidance literature:

With water; In dimethyl sulfoxide; at 36.84 ℃; for 0.5h;

DOI:10.1016/j.ejmech.2014.02.062

upstream raw materials:

6-(2-(2-aminoethylamino)ethoxy)-4-(3-chloro-4-fluoro-phenylamino)-7-methoxy quinazoline

Downstream raw materials:

6-(2-(2-aminoethylamino)ethoxy)-4-(3-chloro-4-fluoro-phenylamino)-7-methoxy quinazoline

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