N-[2-(1-Phenyl-adamantan-2-yl)-ethyl]-2-{N-[2-(1-phenyl-adamantan-2-yl)-ethyl]-carbamimidoylmethyldisulfanyl}-acetamidine; hydrochloride

Base Information

Chemical Name:N-[2-(1-Phenyl-adamantan-2-yl)-ethyl]-2-{N-[2-(1-phenyl-adamantan-2-yl)-ethyl]-carbamimidoylmethyldisulfanyl}-acetamidine; hydrochloride
CAS No.:117077-38-0
Molecular Formula:C₄₀H₅₄N₄S₂*2ClH
Molecular Weight:727.949
Hs Code.:

Synonyms:N-[2-(1-Phenyl-adamantan-2-yl)-ethyl]-2-{N-[2-(1-phenyl-adamantan-2-yl)-ethyl]-carbamimidoylmethyldisulfanyl}-acetamidine; hydrochloride

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Chemical Property of N-[2-(1-Phenyl-adamantan-2-yl)-ethyl]-2-{N-[2-(1-phenyl-adamantan-2-yl)-ethyl]-carbamimidoylmethyldisulfanyl}-acetamidine; hydrochloride

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Technology Process of N-[2-(1-Phenyl-adamantan-2-yl)-ethyl]-2-{N-[2-(1-phenyl-adamantan-2-yl)-ethyl]-carbamimidoylmethyldisulfanyl}-acetamidine; hydrochloride

There total 12 articles about N-[2-(1-Phenyl-adamantan-2-yl)-ethyl]-2-{N-[2-(1-phenyl-adamantan-2-yl)-ethyl]-carbamimidoylmethyldisulfanyl}-acetamidine; hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: S-(N-<2-(1-phenyl-2-adamantyl)ethyl>carboxamidiniummethyl) thiosulfate

: 117077-38-0
N-[2-(1-Phenyl-adamantan-2-yl)-ethyl]-2-{N-[2-(1-phenyl-adamantan-2-yl)-ethyl]-carbamimidoylmethyldisulfanyl}-acetamidine; hydrochloride

Guidance literature:: With hydrogenchloride; thiourea; In isopropyl alcohol; at 95 - 100 ℃; for 10h;
DOI:10.1016/S0040-4020(01)90332-1

Reference yield:

: 27567-85-7
4-protoadamantanone

: 117077-38-0
N-[2-(1-Phenyl-adamantan-2-yl)-ethyl]-2-{N-[2-(1-phenyl-adamantan-2-yl)-ethyl]-carbamimidoylmethyldisulfanyl}-acetamidine; hydrochloride

Guidance literature:: Multi-step reaction with 11 steps

1: tetrahydrofuran / 4 h / Heating

2: 0.5 h / Heating; reflux with 98percent HCOOH

3: 79 percent / 1 N HCl / acetone / 2 h / Heating

4: 87 percent / Jones reagent (CrO₃) / acetone; H₂O / 3.5 h / 15 °C

5: 92 percent / 50 percent NaH in paraffin / tetrahydrofuran / 0.17 h / 25 °C

6: 96 percent / H₂ / 10 percent Pd/C / ethanol / 30 h / 25 °C / 2068.6 Torr

7: 95 percent / 30 percent H₂O₂, 0.2 M aq. NaOH / methanol; dimethylsulfoxide / 12 h / 50 - 55 °C

8: 100 percent / 1.) LiAlH₄ 2.) HCl gas / tetrahydrofuran / 24 h / Heating

9: 95 percent / HCl / methanol / 12 h

10: 89 percent / sodium thiosulfate / methanol; H₂O / 0.5 h / 80 - 85 °C

11: 65 percent / thiourea, 1 N HCl / propan-2-ol / 10 h / 95 - 100 °C

With chromium(VI) oxide; hydrogenchloride; sodium hydroxide; lithium aluminium tetrahydride; hydrogen; dihydrogen peroxide; sodium hydride; sodium thiosulfate; thiourea; palladium on activated charcoal; In tetrahydrofuran; methanol; ethanol; water; dimethyl sulfoxide; isopropyl alcohol; acetone;
DOI:10.1016/S0040-4020(01)90332-1

Reference yield:

: 40571-15-1
1-phenyl-2-adamantanol

: 117077-38-0
N-[2-(1-Phenyl-adamantan-2-yl)-ethyl]-2-{N-[2-(1-phenyl-adamantan-2-yl)-ethyl]-carbamimidoylmethyldisulfanyl}-acetamidine; hydrochloride

Guidance literature:: Multi-step reaction with 8 steps

1: 87 percent / Jones reagent (CrO₃) / acetone; H₂O / 3.5 h / 15 °C

2: 92 percent / 50 percent NaH in paraffin / tetrahydrofuran / 0.17 h / 25 °C

3: 96 percent / H₂ / 10 percent Pd/C / ethanol / 30 h / 25 °C / 2068.6 Torr

4: 95 percent / 30 percent H₂O₂, 0.2 M aq. NaOH / methanol; dimethylsulfoxide / 12 h / 50 - 55 °C

5: 100 percent / 1.) LiAlH₄ 2.) HCl gas / tetrahydrofuran / 24 h / Heating

6: 95 percent / HCl / methanol / 12 h

7: 89 percent / sodium thiosulfate / methanol; H₂O / 0.5 h / 80 - 85 °C

8: 65 percent / thiourea, 1 N HCl / propan-2-ol / 10 h / 95 - 100 °C

With chromium(VI) oxide; hydrogenchloride; sodium hydroxide; lithium aluminium tetrahydride; hydrogen; dihydrogen peroxide; sodium hydride; sodium thiosulfate; thiourea; palladium on activated charcoal; In tetrahydrofuran; methanol; ethanol; water; dimethyl sulfoxide; isopropyl alcohol; acetone;
DOI:10.1016/S0040-4020(01)90332-1