bis-[bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-phosphinic acid 2-(5-methyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-ethyl ester

Base Information

Chemical Name:bis-[bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-phosphinic acid 2-(5-methyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-ethyl ester
CAS No.:473420-76-7
Molecular Formula:C₅₁H₅₁N₂O₁₀P
Molecular Weight:882.947
Hs Code.:

bis-[bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-phosphinic acid 2-(5-methyl-2,4-dioxo-3,4-dihydro-2<i>H</i>-pyrimidin-1-yl)-ethyl ester

Synonyms:bis-[bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-phosphinic acid 2-(5-methyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-ethyl ester

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Chemical Property of bis-[bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-phosphinic acid 2-(5-methyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-ethyl ester

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Technology Process of bis-[bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-phosphinic acid 2-(5-methyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-ethyl ester

There total 3 articles about bis-[bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-phosphinic acid 2-(5-methyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 22441-51-6
N-1-(2-hydroxyethyl)thymine

: bis-[bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-phosphinic acid; compound with tert-butyl-methyl-amine

: 473420-76-7
bis-[bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-phosphinic acid 2-(5-methyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-ethyl ester

Guidance literature:: With pyridine; 1-(mesitylene-2-sulfonyl)-3-nitro-1H-1,2,4-triazole; at 20 ℃; for 24h;
DOI:10.1016/S0040-4039(02)01067-5

Reference yield:

: 40615-36-9
4,4'-dimethoxytrityl chloride

: 473420-76-7
bis-[bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-phosphinic acid 2-(5-methyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-ethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 80 percent / pyridine / 12 h / 20 °C

2: 10 h / 100 °C

3: 75 percent / 1-(2-mesitylensulfonyl)-3-nitro-1,2,4-triazole; pyridine / 24 h / 20 °C

With pyridine; 1-(mesitylene-2-sulfonyl)-3-nitro-1H-1,2,4-triazole;
DOI:10.1016/S0040-4039(02)01067-5

Reference yield:

: 714251-15-7
bis-[bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-phosphinic acid methyl ester

: 473420-76-7
bis-[bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-phosphinic acid 2-(5-methyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-ethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 10 h / 100 °C

2: 75 percent / 1-(2-mesitylensulfonyl)-3-nitro-1,2,4-triazole; pyridine / 24 h / 20 °C

With pyridine; 1-(mesitylene-2-sulfonyl)-3-nitro-1H-1,2,4-triazole;
DOI:10.1016/S0040-4039(02)01067-5