6-(2-chlorophenyl)-7-hydroxy-5,8-diazabenzophenanthrene

Base Information

Chemical Name:6-(2-chlorophenyl)-7-hydroxy-5,8-diazabenzophenanthrene
CAS No.:107428-45-5
Molecular Formula:C₂₂H₁₃ClN₂O
Molecular Weight:356.811
Hs Code.:

6-(2-chlorophenyl)-7-hydroxy-5,8-diazabenzo<c>phenanthrene

Synonyms:6-(2-chlorophenyl)-7-hydroxy-5,8-diazabenzophenanthrene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 6-(2-chlorophenyl)-7-hydroxy-5,8-diazabenzophenanthrene

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Technology Process of 6-(2-chlorophenyl)-7-hydroxy-5,8-diazabenzophenanthrene

There total 1 articles about 6-(2-chlorophenyl)-7-hydroxy-5,8-diazabenzophenanthrene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 606-10-0
2,2'-diaminobenzophenone

: 19112-35-7
ethyl (2-chlorobenzoyl)acetate

: 107428-45-5
6-(2-chlorophenyl)-7-hydroxy-5,8-diazabenzophenanthrene

Guidance literature:: In acetic acid; at 160 ℃; for 1.5h;

Reference yield: 75.0%

: 107428-45-5
6-(2-chlorophenyl)-7-hydroxy-5,8-diazabenzophenanthrene

: 107428-41-1
6-chloro-7-(2-chlorophenyl)-5,8-diazabenzophenanthrene

Guidance literature:: With thionyl chloride; In N,N-dimethyl-formamide; for 2h; Heating;

Reference yield:

: 107428-45-5
6-(2-chlorophenyl)-7-hydroxy-5,8-diazabenzophenanthrene

: 107263-24-1
6-phenyl-5,8-diazabenzophenanthrene

Guidance literature:: Multi-step reaction with 2 steps

1: 75 percent / SOCl₂ / dimethylformamide / 2 h / Heating

2: 48 percent / H₂, KOH / 10percent Pd-C / toluene; ethanol

With potassium hydroxide; thionyl chloride; hydrogen; palladium on activated charcoal; In ethanol; N,N-dimethyl-formamide; toluene;