tert-butyl (3S, αR)-3-[N-( 3'-aminopropyl)-N-(α-methylbenzyl)amino]-3-phenylpropanoate

Base Information

Chemical Name:tert-butyl (3S, αR)-3-[N-( 3'-aminopropyl)-N-(α-methylbenzyl)amino]-3-phenylpropanoate
CAS No.:1393593-25-3
Molecular Formula:C₂₄H₃₄N₂O₂
Molecular Weight:382.546
Hs Code.:

Synonyms:tert-butyl (3S, αR)-3-[N-( 3'-aminopropyl)-N-(α-methylbenzyl)amino]-3-phenylpropanoate

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Chemical Property of tert-butyl (3S, αR)-3-[N-( 3'-aminopropyl)-N-(α-methylbenzyl)amino]-3-phenylpropanoate

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Technology Process of tert-butyl (3S, αR)-3-[N-( 3'-aminopropyl)-N-(α-methylbenzyl)amino]-3-phenylpropanoate

There total 2 articles about tert-butyl (3S, αR)-3-[N-( 3'-aminopropyl)-N-(α-methylbenzyl)amino]-3-phenylpropanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 1393593-24-2
tert-butyl (3S, αR)-3-[N-( 3'-azidopropyl)-N-(α-methylbenzyl)amino]-3-phenylpropanoate

: 1393593-25-3
tert-butyl (3S, αR)-3-[N-( 3'-aminopropyl)-N-(α-methylbenzyl)amino]-3-phenylpropanoate

Guidance literature:: tert-butyl (3S, αR)-3-[N-( 3'-azidopropyl)-N-(α-methylbenzyl)amino]-3-phenylpropanoate; With triphenylphosphine; In tetrahydrofuran; at 20 ℃; for 0.5h;

With water; In tetrahydrofuran; at 50 ℃; for 2h;
DOI:10.1021/jo3012732

Reference yield:

: 1393593-22-0
tert-butyl (3S, αR)-3-[N-( 3'-chloropropyl)-N-(α-methylbenzyl)amino]-3-phenylpropanoate

: 1393593-25-3
tert-butyl (3S, αR)-3-[N-( 3'-aminopropyl)-N-(α-methylbenzyl)amino]-3-phenylpropanoate

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium azide; sodium iodide / dimethyl sulfoxide / 48 h / 50 °C

2.1: triphenylphosphine / tetrahydrofuran / 0.5 h / 20 °C

2.2: 2 h / 50 °C

With sodium azide; triphenylphosphine; sodium iodide; In tetrahydrofuran; dimethyl sulfoxide;
DOI:10.1021/jo3012732