4-bromo-2-cyanophenyl tert-butyl carbonate

Base Information

Chemical Name:4-bromo-2-cyanophenyl tert-butyl carbonate
CAS No.:1169559-70-9
Molecular Formula:C₁₂H₁₂BrNO₃
Molecular Weight:298.136
Hs Code.:

Synonyms:4-bromo-2-cyanophenyl tert-butyl carbonate

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Chemical Property of 4-bromo-2-cyanophenyl tert-butyl carbonate

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Technology Process of 4-bromo-2-cyanophenyl tert-butyl carbonate

There total 1 articles about 4-bromo-2-cyanophenyl tert-butyl carbonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 24424-99-5
di-tert-butyl dicarbonate

: 40530-18-5
5-bromo-2-hydroxybenzonitrile

: 1169559-70-9
4-bromo-2-cyanophenyl tert-butyl carbonate

Guidance literature:: dmap; In hexane; dichloromethane; acetonitrile; at 20 - 50 ℃; for 0.333333h;

Reference yield: 87.0%

: 1169559-70-9
4-bromo-2-cyanophenyl tert-butyl carbonate

: 7486-35-3
tri-n-butyl(vinyl)tin

: 1169559-87-8
tert-butyl 2-cyano-4-vinylphenyl carbonate

Guidance literature:: tetrakis(triphenylphosphine) palladium⁽⁰⁾; In toluene; at 110 ℃; for 6h;

Reference yield: 67.0%

: 1169559-70-9
4-bromo-2-cyanophenyl tert-butyl carbonate

: 411235-57-9
cyclopropylboronic acid

: 1169559-73-2
tert-butyl 2-cyano-4-cyclopropylphenyl carbonate

Guidance literature:: With potassium phosphate; palladium diacetate; tricyclohexylphosphine; In water; toluene;
DOI:10.1016/j.bmcl.2012.04.025