perhydro-3a-(4-nitrobenzyl)-3a,5a,8a,10a-tetraazapyrenium bromide

Base Information

Chemical Name:perhydro-3a-(4-nitrobenzyl)-3a,5a,8a,10a-tetraazapyrenium bromide
CAS No.:1021925-74-5
Molecular Formula:Br*C₁₉H₂₈N₅O₂
Molecular Weight:438.368
Hs Code.:

Synonyms:perhydro-3a-(4-nitrobenzyl)-3a,5a,8a,10a-tetraazapyrenium bromide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of perhydro-3a-(4-nitrobenzyl)-3a,5a,8a,10a-tetraazapyrenium bromide

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Technology Process of perhydro-3a-(4-nitrobenzyl)-3a,5a,8a,10a-tetraazapyrenium bromide

There total 1 articles about perhydro-3a-(4-nitrobenzyl)-3a,5a,8a,10a-tetraazapyrenium bromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 72738-47-7
decahydro-1H,6H-3a,5a,8a,10a-tetraazapyrene

: 100-11-8
1-bromomethyl-4-nitro-benzene

: 1021925-74-5
perhydro-3a-(4-nitrobenzyl)-3a,5a,8a,10a-tetraazapyrenium bromide

Guidance literature:: In acetonitrile; for 48h;
DOI:10.1039/b709747f

Reference yield: 100.0%

: 1021925-74-5
perhydro-3a-(4-nitrobenzyl)-3a,5a,8a,10a-tetraazapyrenium bromide

: 105-36-2
ethyl bromoacetate

: 3BrH*Br^(1-)*C₂₃H₃₆N₅O₆⁽¹⁺⁾

Guidance literature:: perhydro-3a-(4-nitrobenzyl)-3a,5a,8a,10a-tetraazapyrenium bromide; ethyl bromoacetate; With triethylamine; N-ethyl-N,N-diisopropylamine; In acetonitrile; at 20 ℃;

With hydrogenchloride; Heating;

With hydrogen bromide; Further stages.;
DOI:10.1039/b709747f

Reference yield: 100.0%

: 1021925-74-5
perhydro-3a-(4-nitrobenzyl)-3a,5a,8a,10a-tetraazapyrenium bromide

: 5292-43-3
bromoacetic acid tert-butyl ester

: 3BrH*Br^(1-)*C₂₃H₃₆N₅O₆⁽¹⁺⁾

Guidance literature:: perhydro-3a-(4-nitrobenzyl)-3a,5a,8a,10a-tetraazapyrenium bromide; bromoacetic acid tert-butyl ester; With potassium carbonate; In acetonitrile; at 20 ℃;

With trifluoroacetic acid; In dichloromethane; at 20 ℃;

With hydrogen bromide; Further stages.;
DOI:10.1039/b709747f