diisopropyl-phosphoramidous acid 2-cyano-ethyl ester 2-(10,16-dibenzyl-1,7,13-trioxa-4,10,16-triaza-cyclooctadec-4-yl)-ethyl ester

Base Information

Chemical Name:diisopropyl-phosphoramidous acid 2-cyano-ethyl ester 2-(10,16-dibenzyl-1,7,13-trioxa-4,10,16-triaza-cyclooctadec-4-yl)-ethyl ester
CAS No.:587875-00-1
Molecular Formula:C₃₇H₆₀N₅O₅P
Molecular Weight:685.888
Hs Code.:

Synonyms:diisopropyl-phosphoramidous acid 2-cyano-ethyl ester 2-(10,16-dibenzyl-1,7,13-trioxa-4,10,16-triaza-cyclooctadec-4-yl)-ethyl ester

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Chemical Property of diisopropyl-phosphoramidous acid 2-cyano-ethyl ester 2-(10,16-dibenzyl-1,7,13-trioxa-4,10,16-triaza-cyclooctadec-4-yl)-ethyl ester

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Technology Process of diisopropyl-phosphoramidous acid 2-cyano-ethyl ester 2-(10,16-dibenzyl-1,7,13-trioxa-4,10,16-triaza-cyclooctadec-4-yl)-ethyl ester

There total 6 articles about diisopropyl-phosphoramidous acid 2-cyano-ethyl ester 2-(10,16-dibenzyl-1,7,13-trioxa-4,10,16-triaza-cyclooctadec-4-yl)-ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: 124482-92-4,89992-70-1
2-cyanoethyl-N,N-(diisopropylamino)chlorophosphine

: 587874-99-5
2-(10,16-dibenzyl-1,7,13-trioxa-4,10,16-triaza-cyclooctadec-4-yl)-ethanol

: 587875-00-1
diisopropyl-phosphoramidous acid 2-cyano-ethyl ester 2-(10,16-dibenzyl-1,7,13-trioxa-4,10,16-triaza-cyclooctadec-4-yl)-ethyl ester

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In dichloromethane;
DOI:10.1039/b301100c

Reference yield:

: 124243-65-8
N-<2-(2-hydroxyethoxy)ethyl>benzamide

: 587875-00-1
diisopropyl-phosphoramidous acid 2-cyano-ethyl ester 2-(10,16-dibenzyl-1,7,13-trioxa-4,10,16-triaza-cyclooctadec-4-yl)-ethyl ester

Guidance literature:: Multi-step reaction with 5 steps

1: 80 percent / pyridine

2: 70 percent / Et₃N / acetonitrile

3: 90 percent / LiAlH₄ / tetrahydrofuran

4: 50 percent / Na₂CO₃ / acetonitrile

5: 50 percent / EtN(i-Pr)2 / CH₂Cl₂

With pyridine; lithium aluminium tetrahydride; sodium carbonate; triethylamine; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; dichloromethane; acetonitrile;
DOI:10.1081/NCN-120022730

Reference yield:

: 93-97-0
benzoic acid anhydride

: 587875-00-1
diisopropyl-phosphoramidous acid 2-cyano-ethyl ester 2-(10,16-dibenzyl-1,7,13-trioxa-4,10,16-triaza-cyclooctadec-4-yl)-ethyl ester

Guidance literature:: Multi-step reaction with 6 steps

1: 90 percent / ethanol / Heating

2: 80 percent / pyridine

3: 70 percent / Et₃N / acetonitrile

4: 90 percent / LiAlH₄ / tetrahydrofuran

5: 50 percent / Na₂CO₃ / acetonitrile

6: 50 percent / EtN(i-Pr)2 / CH₂Cl₂

With pyridine; lithium aluminium tetrahydride; sodium carbonate; triethylamine; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; ethanol; dichloromethane; acetonitrile;
DOI:10.1081/NCN-120022730