5-methoxy-2-(5-(methoxyimino)-5,6,7,8-tetrahydroquinolin-2-yl)phenyl acetate

Base Information

Chemical Name:5-methoxy-2-(5-(methoxyimino)-5,6,7,8-tetrahydroquinolin-2-yl)phenyl acetate
CAS No.:1477476-40-6
Molecular Formula:C₁₉H₂₀N₂O₄
Molecular Weight:340.379
Hs Code.:

Synonyms:5-methoxy-2-(5-(methoxyimino)-5,6,7,8-tetrahydroquinolin-2-yl)phenyl acetate

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Chemical Property of 5-methoxy-2-(5-(methoxyimino)-5,6,7,8-tetrahydroquinolin-2-yl)phenyl acetate

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Technology Process of 5-methoxy-2-(5-(methoxyimino)-5,6,7,8-tetrahydroquinolin-2-yl)phenyl acetate

There total 4 articles about 5-methoxy-2-(5-(methoxyimino)-5,6,7,8-tetrahydroquinolin-2-yl)phenyl acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 1477476-63-3
C₁₇H₁₈N₂O₂

: 108-24-7
acetic anhydride

: 1477476-40-6
5-methoxy-2-(5-(methoxyimino)-5,6,7,8-tetrahydroquinolin-2-yl)phenyl acetate

Guidance literature:: With [bis(acetoxy)iodo]benzene; palladium diacetate; In acetonitrile; at 100 ℃; for 6h; regioselective reaction; Inert atmosphere;
DOI:10.1039/c3ra41312h

Reference yield:

: 59838-66-3
2-(4-methoxyphenyl)-7,8-dihydroquinolin-5(6H)-one

: 1477476-40-6
5-methoxy-2-(5-(methoxyimino)-5,6,7,8-tetrahydroquinolin-2-yl)phenyl acetate

Guidance literature:: Multi-step reaction with 2 steps

1: sodium acetate / water; ethanol / 2 h / 70 °C

2: palladium diacetate; [bis(acetoxy)iodo]benzene / acetonitrile / 6 h / 100 °C / Inert atmosphere

With [bis(acetoxy)iodo]benzene; sodium acetate; palladium diacetate; In ethanol; water; acetonitrile;
DOI:10.1039/c3ra41312h

Reference yield:

: 100-06-1
1-(4-methoxyphenyl)ethanone

: 1477476-40-6
5-methoxy-2-(5-(methoxyimino)-5,6,7,8-tetrahydroquinolin-2-yl)phenyl acetate

Guidance literature:: Multi-step reaction with 4 steps

1: N,N-dimethyl acetamide; toluene / 7 h / Reflux

2: sodium iodide; cerium(III) chloride heptahydrate; ammonium acetate / isopropyl alcohol / 4 h / Reflux

3: sodium acetate / water; ethanol / 2 h / 70 °C

4: palladium diacetate; [bis(acetoxy)iodo]benzene / acetonitrile / 6 h / 100 °C / Inert atmosphere

With [bis(acetoxy)iodo]benzene; cerium(III) chloride heptahydrate; ammonium acetate; sodium acetate; palladium diacetate; sodium iodide; In ethanol; N,N-dimethyl acetamide; water; isopropyl alcohol; toluene; acetonitrile;
DOI:10.1039/c3ra41312h