Technology Process of C39H54N6O5Si
There total 5 articles about C39H54N6O5Si which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; potassium phosphate; tris-(dibenzylideneacetone)dipalladium(0);
In
1,4-dioxane; water;
at 80 ℃;
for 2h;
Inert atmosphere;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: sodium t-butanolate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; palladium diacetate / 1,2-dimethoxyethane / 5 h / Inert atmosphere; Reflux
2.1: trichlorophosphate / 0.67 h / 80 °C
3.1: sodium hydride / N,N-dimethyl-formamide / 1 h / 5 °C / Inert atmosphere
3.2: 5 h / 5 - 20 °C / Inert atmosphere
4.1: potassium phosphate; dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; tris-(dibenzylideneacetone)dipalladium(0) / 1,4-dioxane; water / 2 h / 80 °C / Inert atmosphere
With
dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; potassium phosphate; tris-(dibenzylideneacetone)dipalladium(0); palladium diacetate; sodium hydride; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; sodium t-butanolate; trichlorophosphate;
In
1,4-dioxane; 1,2-dimethoxyethane; water; N,N-dimethyl-formamide;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: sodium t-butanolate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; palladium diacetate / 1,2-dimethoxyethane / 5 h / Inert atmosphere; Reflux
2.1: trichlorophosphate / 0.67 h / 80 °C
3.1: sodium hydride / N,N-dimethyl-formamide / 1 h / 5 °C / Inert atmosphere
3.2: 5 h / 5 - 20 °C / Inert atmosphere
4.1: potassium phosphate; dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; tris-(dibenzylideneacetone)dipalladium(0) / 1,4-dioxane; water / 2 h / 80 °C / Inert atmosphere
With
dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; potassium phosphate; tris-(dibenzylideneacetone)dipalladium(0); palladium diacetate; sodium hydride; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; sodium t-butanolate; trichlorophosphate;
In
1,4-dioxane; 1,2-dimethoxyethane; water; N,N-dimethyl-formamide;