methyl 5-chloro-3-[ethyl(1-methylpiperidin-4-yl)amino]-2-methylbenzoate

Base Information

Chemical Name:methyl 5-chloro-3-[ethyl(1-methylpiperidin-4-yl)amino]-2-methylbenzoate
CAS No.:1403595-33-4
Molecular Formula:C₁₇H₂₅ClN₂O₂
Molecular Weight:324.851
Hs Code.:

Synonyms:methyl 5-chloro-3-[ethyl(1-methylpiperidin-4-yl)amino]-2-methylbenzoate

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Chemical Property of methyl 5-chloro-3-[ethyl(1-methylpiperidin-4-yl)amino]-2-methylbenzoate

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Technology Process of methyl 5-chloro-3-[ethyl(1-methylpiperidin-4-yl)amino]-2-methylbenzoate

There total 6 articles about methyl 5-chloro-3-[ethyl(1-methylpiperidin-4-yl)amino]-2-methylbenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 50-00-0,30525-89-4,61233-19-0
formaldehyd

: C₂HF₃O₂*C₁₆H₂₃ClN₂O₂

: 1403595-33-4
methyl 5-chloro-3-[ethyl(1-methylpiperidin-4-yl)amino]-2-methylbenzoate

Guidance literature:: formaldehyd; C₂HF₃O₂*C₁₆H₂₃ClN₂O₂; With sodium tris(acetoxy)borohydride; acetic acid; In tetrahydrofuran; water; at 23 ℃; for 19h;

With sodium hydrogencarbonate; In tetrahydrofuran; water;

Reference yield:

: 79099-07-3
N-tert-butyloxycarbonylpiperidin-4-one

: 1403595-33-4
methyl 5-chloro-3-[ethyl(1-methylpiperidin-4-yl)amino]-2-methylbenzoate

Guidance literature:: Multi-step reaction with 4 steps

1.1: acetic acid; sodium tris(acetoxy)borohydride / dichloromethane / 18 h / 23 °C

2.1: acetic acid / 1,2-dichloro-ethane / 0.08 h / 20 °C / Inert atmosphere

2.2: 22.5 h / 20 °C

3.1: dichloromethane / 2 h / 20 °C

4.1: acetic acid; sodium tris(acetoxy)borohydride / water; tetrahydrofuran / 19 h / 23 °C

With sodium tris(acetoxy)borohydride; acetic acid; In tetrahydrofuran; dichloromethane; water; 1,2-dichloro-ethane;

Reference yield:

: 154257-81-5
5-chloro-2-methyl-3-nitrobenzoic acid

: 1403595-33-4
methyl 5-chloro-3-[ethyl(1-methylpiperidin-4-yl)amino]-2-methylbenzoate

Guidance literature:: Multi-step reaction with 6 steps

1.1: sodium carbonate / N,N-dimethyl-formamide / 4 h / 60 °C

2.1: water; ammonium chloride; iron / ethanol / 1 h / 80 °C

3.1: acetic acid; sodium tris(acetoxy)borohydride / dichloromethane / 18 h / 23 °C

4.1: acetic acid / 1,2-dichloro-ethane / 0.08 h / 20 °C / Inert atmosphere

4.2: 22.5 h / 20 °C

5.1: dichloromethane / 2 h / 20 °C

6.1: acetic acid; sodium tris(acetoxy)borohydride / water; tetrahydrofuran / 19 h / 23 °C

With water; sodium tris(acetoxy)borohydride; iron; sodium carbonate; ammonium chloride; acetic acid; In tetrahydrofuran; ethanol; dichloromethane; water; 1,2-dichloro-ethane; N,N-dimethyl-formamide;