(Z)-tert-butyl (2-(5-(4-ethoxybenzylidene)-2,4-dioxothiazolidin-3-yl)propyl)carbamate

Base Information

Chemical Name:(Z)-tert-butyl (2-(5-(4-ethoxybenzylidene)-2,4-dioxothiazolidin-3-yl)propyl)carbamate
CAS No.:1438409-77-8
Molecular Formula:C₂₀H₂₆N₂O₅S
Molecular Weight:406.503
Hs Code.:

Synonyms:(Z)-tert-butyl (2-(5-(4-ethoxybenzylidene)-2,4-dioxothiazolidin-3-yl)propyl)carbamate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (Z)-tert-butyl (2-(5-(4-ethoxybenzylidene)-2,4-dioxothiazolidin-3-yl)propyl)carbamate

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Technology Process of (Z)-tert-butyl (2-(5-(4-ethoxybenzylidene)-2,4-dioxothiazolidin-3-yl)propyl)carbamate

There total 3 articles about (Z)-tert-butyl (2-(5-(4-ethoxybenzylidene)-2,4-dioxothiazolidin-3-yl)propyl)carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 15.4%

: 121102-88-3
tert-butyl N-(2-bromopropyl)carbamate

: (Z)-5-(4-ethoxybenzylidene)thiazolidine-2,4-dione

: 1438409-77-8
(Z)-tert-butyl (2-(5-(4-ethoxybenzylidene)-2,4-dioxothiazolidin-3-yl)propyl)carbamate

Guidance literature:: (Z)-5-(4-ethoxybenzylidene)thiazolidine-2,4-dione; With potassium carbonate; In N,N-dimethyl-formamide; at 0 ℃; for 0.333333h;

tert-butyl N-(2-bromopropyl)carbamate; In N,N-dimethyl-formamide; at 20 ℃; for 0.3h;
DOI:10.1039/c3ob40199e

Reference yield: 15.4%

: 1438409-77-8
(Z)-tert-butyl (2-(5-(4-ethoxybenzylidene)-2,4-dioxothiazolidin-3-yl)propyl)carbamate

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 0 ℃; for 0.333333h; Inert atmosphere;

In N,N-dimethyl-formamide; at 20 ℃; for 3h; Inert atmosphere;

Reference yield:

: 10031-82-0
4-ethoxybenzaldehyde

: 1438409-77-8
(Z)-tert-butyl (2-(5-(4-ethoxybenzylidene)-2,4-dioxothiazolidin-3-yl)propyl)carbamate

Guidance literature:: Multi-step reaction with 2 steps

1.1: piperidine / ethanol / 24 h / 20 - 75 °C

2.1: potassium carbonate / N,N-dimethyl-formamide / 0.33 h / 0 °C

2.2: 0.3 h / 20 °C

With piperidine; potassium carbonate; In ethanol; N,N-dimethyl-formamide; 1.1: |Knoevenagel Condensation;
DOI:10.1039/c3ob40199e