dithiocarbonic acid S-[2-(4-tert-butyl-phenyl)-4-oxo-cyclobutyl] ester O-(2,2-dimethyl-propyl) ester

Base Information

• Chemical Name: dithiocarbonic acid S-[2-(4-tert-butyl-phenyl)-4-oxo-cyclobutyl] ester O-(2,2-dimethyl-propyl) ester
• CAS No.: 627900-67-8
• Molecular Formula: C₂₀H₂₈O₂S₂
• Molecular Weight: 364.573

Synonyms:dithiocarbonic acid S-[2-(4-tert-butyl-phenyl)-4-oxo-cyclobutyl] ester O-(2,2-dimethyl-propyl) ester

Chemical Property of dithiocarbonic acid S-[2-(4-tert-butyl-phenyl)-4-oxo-cyclobutyl] ester O-(2,2-dimethyl-propyl) ester

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Technology Process of dithiocarbonic acid S-[2-(4-tert-butyl-phenyl)-4-oxo-cyclobutyl] ester O-(2,2-dimethyl-propyl) ester

There total 1 articles about dithiocarbonic acid S-[2-(4-tert-butyl-phenyl)-4-oxo-cyclobutyl] ester O-(2,2-dimethyl-propyl) ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

sodium O-neopentyl xanthate salt + 2-bromo-3-(4-tert-butyl-phenyl)-cyclobutanone → dithiocarbonic acid S-[2-(4-tert-butyl-phenyl)-4-oxo-cyclobutyl] ester O-(2,2-dimethyl-propyl) ester (627900-67-8)

Guidance literature:

In acetone; at 20 ℃; for 5h;

DOI:10.1016/j.tetlet.2003.09.042

Reference yield: 76.0%

N-tert-butoxycarbonylprop-2-en-1-amine (78888-18-3) + dithiocarbonic acid S-[2-(4-tert-butyl-phenyl)-4-oxo-cyclobutyl] ester O-(2,2-dimethyl-propyl) ester (627900-67-8) → dithiocarbonic acid S-{1-(tert-butoxycarbonylamino-methyl)-2-[2-(4-tert-butyl-phenyl)-4-oxo-cyclobutyl]-ethyl} ester O-(2,2-dimethyl-propyl) ester (627900-96-3)

Guidance literature:

With dilauryl peroxide; In 1,2-dichloro-ethane; Heating;

DOI:10.1016/j.tetlet.2003.09.042

Reference yield:

N-tert-butoxycarbonylprop-2-en-1-amine (78888-18-3) + dithiocarbonic acid S-[2-(4-tert-butyl-phenyl)-4-oxo-cyclobutyl] ester O-(2,2-dimethyl-propyl) ester (627900-67-8) → {3-[2-(4-tert-butyl-phenyl)-4-oxo-cyclobutyl]-propyl}-carbamic acid tert-butyl ester + {3-[2-(4-tert-butyl-phenyl)-4-oxo-cyclobutyl]-propyl}-carbamic acid tert-butyl ester

Guidance literature:

Multi-step reaction with 2 steps

1: dilauryl peroxide / 1,2-dichloro-ethane / Heating

2: 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride / cyclohexane; toluene / Heating

With 2,2'-azobis(isobutyronitrile); dilauryl peroxide; tri-n-butyl-tin hydride; In cyclohexane; 1,2-dichloro-ethane; toluene;

DOI:10.1016/j.tetlet.2003.09.042

Downstream raw materials:

dithiocarbonic acid S-{1-(tert-butoxycarbonylamino-methyl)-2-[2-(4-tert-butyl-phenyl)-4-oxo-cyclobutyl]-ethyl} ester O-(2,2-dimethyl-propyl) ester

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